Laboratory report documenting GCMS analysis of a method blank for sample AE03510 to verify analytical system cleanliness.
NYC-WTC_000037680–000037699Folder label: “GCMS X 2/19/02 A 3/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02MAR08\03510.D Vial: 6 Acq On : 8 Mar 2002 2:46 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 Pyrimidinetetramine- $$ Pyr... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 13.38 0.06 ug/L 48154 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74- 2 2,5-Cyclohexadiene-1,4-dione, 2,... 140 C6H404 000615-94- 6 3 lH,5H-Pyrazolo[l,2-a]pyrazole-l,... 140 C6H8N2O2 019720-72- 4 l-Oxetan-2-one, 4,4-diethyl-3-me... 140 C8H12O2 000000-00-0 50 Abundance Scan 886 (13.376 min): 03510.D(-) m/z 140.00 100.00% 140
5000
54 70 86 94 TT T / A T If 13.00 13.20 13.40 13.60 13.80 01 ■ i ■ ■ ■ ■ i • ■ ■ ■ i ■ • ■ ■ i ----- • 1 ’.1 m/z 70.00 11.69% miz-> 20 30 40 50I 60 70 80 «) 100 110 120 130 140 Abundance #35040: Pyrimidinetetramine- $$ Pyrimidine, 2,4,5,6-tetraa... 1-0
5000 * i * * 1 A A 1- 13.00 13.20 13.40 13.60 13.80 44 71 123 m/z 54.00 11.22% 86 96 112 Of ■ । • i ■ > • • i 1 ' 1 1 ‘ ' I ' ‘ ....... - miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35122: 2,5-Cyclohexadiene-1,4-dione, 2,5-dihydroxy- $$ p-... 1-0
•3.00 13.20 13.40 13.60 13.80 5000 m/z 66.10 11.16% 42 71 fl 53 84 112 94 l-r-r — 0 ' I ' ' ' ' I ' ' ‘ ‘ I TImyur -PP -T miz-> 2b 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35166:1H,5H-Pyrazolo[1,2-a]pyrazole-1,5-dione, tetrahydro- 1-0 13.00 13.20 13.40 13.60 13.80 55 m/z 141.00 9.84% 5000 42 98 27 70 86 112 0 ■ i ■ ■1 ■ i • ■ ■ ■ i ‘' I ‘ ' 1 i ■ ■ - T’I mfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 13.00 13.20 13.40 13.60 13.80
03510.D HP022102.M Fri Mar 15 10:09:05 2002 Page 13
NYC-WTC_000037696
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NYC-WTC_000037660
Laboratory report documenting GCMS analysis of a method blank for sample AE03509 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037635
Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037760
Laboratory report documenting GCMS analysis of a method blank for sample AE03615 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037720
Laboratory report documenting GCMS analysis of a method blank for sample AE03612 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037780
Gas chromatography-mass spectrometry analysis of sample AE03616 performed on 3/28/2002, detecting other unknown compounds with surrogate 2,4-DDD at 5.0 µg detection limit.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037740
Laboratory report documenting GCMS analysis of a method blank for sample AE03614 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037800
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03617 conducted on March 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037700
Laboratory report documenting GCMS analysis of a method blank for sample AE03611 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004494
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010967
Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010887
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052128
Laboratory report showing GCMS analysis of sample AE00843 including surrogate recovery and unknown compounds.
1 shared topics · similarity 0.997
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Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
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