DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\5973N\02FEB01\31219.D Vial: 5 Acq On : 1 Feb 2002 6:03 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L **************************************** ** * * * * * ****** * *** ** * * ******** Peak Number 7 Pyrimidinetetramine- $$ Pyr... Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

13.37 0.04 ug/L 25109 Naphthalene-d8 13.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 78 2 l-Oxetan-2-one, 4,4-diethyl-3-me... 140 C8H1202 000000-00-0 64 3 2-Methoxy-3 -hydrazinyl-pyrazine 140 C5H8N4O 000000-00-0 64 41H,5H-Pyrazolo[1,2-a]pyrazole-1,... 140 C6H8N2O2 019720-72-0 50 Abundance Scan 876 (13.375 min): 31219.D (-) m/z 140.10 100.00% 140

5000

49 70 86 94 13.00 13.20 13.40 13.60 13.80 -- m/ z 70.00 15.53% o‘l ■ ■ ■. I ■ 1II m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35040: Pyrimidinetetramine- $$ Pyrimidine, 2,4,5,6-tetraa... 1-0

5000- 13.00 13.20 13.40 13.60 13.80 44 71 123 m/z 141.00 11.37% 112 86 96 --------------- 0V TTI m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35765: 1-Oxetan-2-one, 4,4-diethyl-3-methylene- 79 140 39 67 13.00 13.20 13.40 13.60 13.80 125 5000 53 111 m/ Z 86.00 10.65% 97

0 0 ■। I......... ■ 1 । mfe-> Abundance 30 40 50 60 70 80 90 100 110 120 #35089:2-Methoxy-3-hydrazinyl-pyrazine 130 140 1 wV y Mwwyw w 1-0 13.00 13.20 13.40 13.60 13.80 m/z 94.10 10.29%

5000 42 A 54 68 80 95 108 121 O-P ■ - i ■ ■ ■ i ■ ' Il ... I I 1di /z—> 30 40 50 60 70 80 90 100 110 120 130 140 13.00 13.20 13.40 13.60 13.80

31219.D SCAN508.M Mon Feb 04 08:41:49 2002 Page 9

NYC-WTC_000004043