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GCMS blank results for sample AE03510, March 28, 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of a method blank for sample AE03510 to verify analytical system cleanliness.

NYC-WTC_000037680–000037699

Folder label: “GCMS X 2/19/02 A 3/8/02

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Scanned page image, NYC-WTC_000037697
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02MAR08\03510.D Vial: 6 Acq On : 8 Mar 2002 2:46 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.11 ug/L 99358 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qua l 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 _____ ____ 9 3 2,4-Diamino-6-(hydroxymethyl)pte... 192 C7H8N60 000945-24-4 53 4 Phenanthrene, 1-methyl- 192 C15H12 000832-69-9 53 Abundance Scan 1675 (22.283 min): 03510.D(-) m/z 192.00 100.00% 192

5000

• • i • ■ • ■ । r • 82 96 146 160 22.00 22.20 22.40 22.60 66 i 118 ll | > I I l>| I I > I | I I I I | I I I I I! 1 49 ’1Tm 0 ’’11’0211901010 mHm r 4 m/z 191.00 18.20% miz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588: 4-METHOXY-BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 5000 22.00 22.20 22.40 22.60 146 175 m/z 193.00 14.33% 0 "‘ITE1‘0‘TETT‘‘1‘11111112111211/111117T T’IU—nutuT 11‘‘111111117 H m/z—> 2030405060 70 8090 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 1512 - ■ I ' ■ ■ ■ I' 22.00 22.20 22.40 22.60 5000 82 m/z 146.00 14.06% 54 110 30 1 94 160 m/z—> 0 T I “ ’1 i —HP TOImmupugt 11]r 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 130 200 Abundance #102009:2,4-Diamino-6-(hydroxymethyl)pteridine $$ 6-Pteri... T T 163 192 _ 22.00 22.20 22.40 22.60 m/z 96.00 13.73% 5000

66 ... 146 176 121 134

m/z—> 0 "TTT1TT’’1’’1111111113 QT n I | i M TI’T TIE") lll 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ■■■i ■ ' 1 I ■ ' ' 1 1 11 1 I • • ■ ■ i ■ 22.00 22.20 22.40 22.60

03510.D HP022102.M Fri Mar 15 10:09:05 2002 Page 14

NYC-WTC_000037697

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NYC-WTC_000037697Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.998

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