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← Document results/DEP Box 23/GCMS X 2/19/02 A 3/8/02
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GCMS blank results for sample AE03510, March 28, 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of a method blank for sample AE03510 to verify analytical system cleanliness.

NYC-WTC_000037680–000037699

Folder label: “GCMS X 2/19/02 A 3/8/02”

←Page 16 of 20→
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02MAR08\03510.D Vial: 6 Acq On : 8 Mar 2002 2:46 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ******************************************************** *,* *********** Peak Number 10 Cyclopentasiloxane, decamet... Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 12.54 0.06 ug/L 43692 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 83 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 83 3 Benzeneethanamine, N-[(pentafluo... 475 C21H26F5NO2Si2 055429-85-1 33 4 3,4-DIHYDROXYMANDELIC ACID-TETRATMS 472 C20H4005Si4 000000-00-0 32 Abundance Scan 812 (12.540 min): 03510.D (-) m/z 73.00 100.00% 73

5000

43 12.20 12.40 12.60 'l2.‘80 ' 0 1 1mmmpe nmm mP Pmmmp m/z 266.90 41.00% miz-> 40 eo 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 t J l 5000 12.20 12.40 12.60 12.80 m/z 355.00 36.91%

miz-> , , 0 TIWODamuUuuupp 191207 251 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 -34 Abundance #313065: Cyclopentasiloxane, decamethyl- 73 "I8 T -n-[ VTTT T T ! > > f 12.20 12.40 12.60 12.80 5000 267 m/z 356.00 13.12% 355 45 193 223 251 k I i r TTTT UTTIWTITITTWTPUI 323339 1 O TI—Tg TT TIUTT 11—0010011001 11] miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #362614: Benzeneethanamine, N-[(pentafluorophenyl)methylen... TV- IT T I 1 ' ‘ ' I ’ ‘ ‘ I 73 12.20 12.40 12.60 12.80 m/z 268.00 10.12%

5000 267 44 |, 151 179194299 250 0- TT ‘I—Buu‘1———TTT TTTT TT IJ , ITT TIUTITT • ■ i"'1 i ■'111'11' 111 ■11 ■ 1 • i ‘ 1 • 1 i • • I ' ■ ' ' i ■ ■ ■ • i m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 12.20 12.40 12.60 12.80

03510.D HP022102.M Fri Mar 15 10:09:05 2002 Page 12

NYC-WTC_000037695

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NYC-WTC_000037695Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.998

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