Laboratory report documenting GCMS analysis of a method blank for sample AE03615 to verify analytical system cleanliness.
NYC-WTC_000037760–000037779Folder label: “GCMS X 2/19/02 A 3/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02MAR08\03615.D Vial: 5 Acq On : 8 Mar 2002 6:52 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 Cyclopentasiloxane, decamet... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 12.54 0.07 ug/L 46173 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 74 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 50 3 3,4-DIHYDROXYMANDELIC ACID-TETRATMS 472 C20H4005Si4 000000-00-0 38 4 N-(Trifluoroacetyl)-N,O,O' ,O''-t... 553 C22H42F3NO4Si4 000000-00-0 37 Abundance Scan 812 (12.540 min): 03515.D (-) m/z 73.00 100.00% 73
5000 267 355 ------- 43 12.20 12.40 12.60 12.80 oUm ■ i ■ ' • ■ i • ■ • ■ i • m/z 266.90 49.74% miz-> 50 100 150 200 250 300 350 400 450 Abundance #313068: Cyclopentasiloxane, decamethyl- 73
355 267 5000 12.20 1240 12.60 1280 1 m/z 355.00 38.76% .............................. — 323.1..... 0+ I 100 150 200 250 300 miz-> 50 350 400 450 Abundance #313065: Cyclopentasiloxane, decamethyl- 73 ■ * ! ‘ ‘ 1 1 » • i ■ ■ ‘ ■ i 1 1 ■ 1 i 12.20 12.40 12.60 12.80 5000 267 m/z 356.00 16.81% 355 45 193 223 , 323 , 01 — - ■ — r 1 r ■ ■ 1 1 — ■ 1 ■ 1 I" 1 1 1 1 1 1 1 miz—> 50 100 150 200 250 300 350 400 450 Abundance #361636: 3,4-DIHYDROXYMANDELIC ACID-TETRATMS ' 1 I 111 1 1 ' 1 i ■ ■ ■ ‘ i ' 1 1 1 i 73 12.20 12.40 12.60 12.80 m/z 267.90 13.57% 355 5000
45 147 0 — j 193 267 295 429 457 1 r -1 TT-j-r-r-r-r-p-r I ' 1 ' 1 I ‘ ‘ ‘ 1 I m/z-> 50 100 150 200 250 300 350 400 450 12.20 12.40 12.60 12.80
03515.D HP022102.M Fri Mar 15 10:09:30 2002 Page 13
NYC-WTC_000037776
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NYC-WTC_000037800
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03617 conducted on March 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037740
Laboratory report documenting GCMS analysis of a method blank for sample AE03614 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037780
Gas chromatography-mass spectrometry analysis of sample AE03616 performed on 3/28/2002, detecting other unknown compounds with surrogate 2,4-DDD at 5.0 µg detection limit.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037635
Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037660
Laboratory report documenting GCMS analysis of a method blank for sample AE03509 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037680
Laboratory report documenting GCMS analysis of a method blank for sample AE03510 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037720
Laboratory report documenting GCMS analysis of a method blank for sample AE03612 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037700
Laboratory report documenting GCMS analysis of a method blank for sample AE03611 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052128
Laboratory report showing GCMS analysis of sample AE00843 including surrogate recovery and unknown compounds.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010027
GCMS laboratory results for sample AE01510 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004494
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010967
Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.
1 shared topics · similarity 0.998
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Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
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