GCMS blank results for sample AE03615, March 28, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02MAR08\03615.D Vial: 5 Acq On : 8 Mar 2002 6:52 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 2-Hydroxy-5-nitropyridine $... Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 13.38 0.05 ug/L 34458 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hydroxy-5-nitropyridine $$ 5-N... 140 C5H4N2O3 005418-51-9/50 2 l-Oxetan-2-one, 4,4-diethyl-3-me... 140 C8H12O2 000000-00-0 9 3 2,5-Cyclohexadiene-1,4-dione, 2,... 140 C6H404 000615-94-1 9 4 3-NITRO-4-HYDROXYPYRIDIN 140 C5H4N2O3 000000-00-0 7 Abundance Scan 886 (13.376 min): 03515.D (-) m/z 140.00 100.00% 140

5000

■ i ■ ■ ■ ■ i ‘ *■ i • 1 1 * r^^ ’ r* 54 70 94 13.00 13.20 13.40 13.60 13.80 44 | — 0! 1 1 1 1 I 1 •htt’ ttT — ..... 108 1 r-r-T m/z 70.00 11.93% miz-> 30 40I 50 60 70 80 90 100 110 120 130 140 Abundance #35063: 2-Hydroxy-5-nitropyridine $$ 5-Nitro-2-hydroxypyri... 1-0

5000 66 ■ i ■ ‘ —A.. .... . 13.00 13.20 13.40 13.60 13.80 m/z 94.00 11.51% 80 93 110 49 * * ’ • i - - 124 I 0- I ‘ ’ 1 1 ’ * ------------ ’tI m/z—> 30 40 50 60I 70 80 90 100 110 120 130 140 Abundance #35765: 1-Oxetan-2-one, 4,4-diethyl-3-methylene- 79 1-0 39 67 —1—/ 13.00 13.20 13.40 13.60 13.80 125 5000 53 111 m/z 54.00 10.09% 97

0 ----- 1 TTI miz—> Abundance 30 40 50 60 70 80 90 00 110 120 130 #35122: 2,5-Cyclohexadiene-1,4-dione, 2,5-dihydroxy- $$ p-.„ 140

1-0 4......... . 13.00 13.20 13.40 13.60 13.80 m/z 141.00 8.41%

5000 42 71 53 84 94 112 0-T 1 1 i 11 1 1 i 1 1 13—1 ■ — - — T m/z—> 30 40 50 60 701 80 90 100 110 120 130 140 13.00 13.20 13.40 13.60 13.80

03515.D HP022102.M Fri Mar 15 10:09:31 2002 Page 14

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