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GCMS analysis results for sample AE01508, Mar 2002

Machine-extracted title · confidence 100%

Analytical results for sample AE01508 analyzed via GCMS on March 4, 2002, including surrogate recovery data.

NYC-WTC_000009966–000009985

Folder label: “GCMS X 1/23/02 A 2/21/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report -* Data File : C:\MSDCHEM\1\5973N\02FEB21\01507.D vial: 4 Acq On : 21 Feb 2002 1:24 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 2,5-Cyclohexadiene-l,4-dion. .. Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

13.38 0.06 ug/L 46064 Naphthalene-d8 13.20

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2,5-Cyclohexadiene-1,4-dione, 2,... 140 C6H404 000615-94-1 53 2 2-Hydroxy-5-nitropyridine $$ 5-N... 140 C5H4N2O3 005418-51-9 40 3 2-Methoxy-3-hydrazinyl-pyrazine 140 C5H8N40 000000-00-0 36 4 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 36 Abundance Scan 886 (13.376 min): 01507.D (-) m/z 140.00 100.00% 140

5000

96 ob 44 52 59 T 84 ' ■ l " ■ p .......... .. "II 13 00 13.20 13.40 13.60 13.80 m/z 66.00 14.28% nz-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35122:2,5-Cyclohexadiene-1,4-dione, 2,5-dihydroxy- $$ p-... 140

......... ....................................... 5000 42 71 13.00 13.20 13.40 13.60 13.80 m/z 96.10 12.94% 53 84 94 112 0]-. - - 1 * i ■ ‘l1 miz-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35063:2-Hydroxy-5-nitropyridine $$ 5-Nitro-2-hydroxypyri... VO • i ■ • **14* • * 1 11*14 13.00 13.20 13.40 13.60 13.80 5000 m/z 70.10 12.18% 66

80 93 110 Oh ..... 49...... , ..... 1......1 —TP 124 I ■ 1 i 1 ' ' ‘ i 1 1 ‘ ‘ I ' 1 TIT n/z—> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35089:2-Methoxy-3-hydrazinyl-pyrazine VO ... .4........ . 13.00 13.20 13.40 13.60 13.80 m/z 141.00 11.40%

5000 42 54 68 80 95 108 121 0[ .... | I • • i • ■ ■ i 1 ■ ...... II....... .1. .I..,.. | kirT ■ • i ■ ■ 1 ‘ i ■ n/z—> 30 40 50 60 70 80 90 100 110 120 130 140 13,00 13.20 13.40 13.60 13,80

01507.D HP022102.M Mon Feb 25 10:54:51 2002 Page 10

NYC-WTC_000009979

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NYC-WTC_000009979Source: NYC Law Department, mirrored locally

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