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GCMS analysis results for sample AE01508, Mar 2002

Machine-extracted title · confidence 100%

Analytical results for sample AE01508 analyzed via GCMS on March 4, 2002, including surrogate recovery data.

NYC-WTC_000009966–000009985

Folder label: “GCMS X 1/23/02 A 2/21/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report -• Data File : C:\MSDCHEM\l\5973N\02FEB21\01507 .D Vial: 4 Acq On : 21 Feb 2002 1:24 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 9 4H-Pyran-4-one, 2-ethyl-3-h... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T.

16.55 0.04 ug/L 29994 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4H-Pyran-4-one, 2-ethyl-3-hydrox. .. 140 C7H803 004940-11-8 25 2 2,5-Cyclohexadiene-1,4-dione, 2,... 140 C6H4O4 000615-94-1 17 3 1,3,5,7-Tetraazatricyclo[3.3.1.1... 140 C6H12N4 000100-97-0 9 4 2,5-Cyclohexadiene-1,4-dione, 2,... 140 C6H404 000615-94-1 9 Abundance Scan 1167 (16.548 min): 01507.D (-) m/z 140.10 100.00% 140

5000 43 71 122 172 56 89 TT 16.20 16.40 16.60 16.80 - evP >. I 4+4 11 > m/z 71.10 33.62% 01 ' i ■ ■ ■ • i • ■ ■ ‘ i 11.8 ■ • i • ‘ ■ i1 ■ ■ ■ i 1111 nz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35346: 4H-Pyran-4-one, 2-ethyl-3-hydroxy- (CAS) $$ Ethyl... 1-0

5000 97 71 16.20 16.40 16.60 16.80 125 m/z 122.10 30.86% 53 84 111 01 ........... 1....... |,I, •. ।. • •. i • >. > । i • I < " 1111 " 111 v — ■ I » । . " i"111 “ i"1' i1 n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35122:2,5-Cyclohexadiene-1,4-dione, 2,5-dihydroxy- $$ p-... 140 16.20 16.40 16.60 16.80 5000 42 m/z 43.00 30.54% 71 53 84 112

miz-> 01 -rT-p 40 50 LL 1TT 1 94 mP4 i * 1 • * r* ' * * । * • * * । * • 60 70 80 90 100 110 120 130 140 150 160 170 mpmmp Abundance #35203:1,3,5,7-Tetraazatricyclo[3.3.1.1(3,7)]decane (CAS)... T 140 16.20 16.40 16.60 16.80 m/z 172.20 30.18% 85 50)0 112 71 0- .......58.1 — ‘ • i ‘ |. 96 ■ i ■ ■ ■11 ■ ■ ‘ ‘ i ‘ -n-p-r-TT-pn- Immmmmmp m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 16.20 16.40 16.60 16.80

01507.D HP022102.M Mon Feb 25 10:54:51 2002 Page 11

NYC-WTC_000009980

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NYC-WTC_000009980Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.998

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