Laboratory report documenting GCMS analysis of a method blank for sample AE03614 to verify analytical system cleanliness.
NYC-WTC_000037740–000037759Folder label: “GCMS X 2/19/02 A 3/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02MAR08\03614.D Vial: 4 Acq On : 8 Mar 2002 6:03 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 Pyridine, 4-nitro-, 1-oxide... Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 13.38 0.05 ug/L 31412 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Pyridine, 4-nitro-, 1-oxide (CAS... 140 C5H4N2O3 001124-33-0 45 2 2-Hydroxy-5-nitropyridine $$ 5-N... 140 C5H4N2O3 005418-51-942 3 2,5-Cyclohexadiene-1,4-dione, 2,... 140 C6H404 000615-94-1 40 4 2,5-Cyclohexadiene-l,4-dione, 2,... 140 C6H404 000615-94-1 40 Abundance Scan 886 (13.376 min): 03514.D (-) m/z 140.00 100.00% 1-0
5000
70' 13.00 13.20 13.40 13.60 13.80 44 54 86 94 108 01 —.......... - ----- । । । [ । 1 m/ z 69.90 12.86% TTT miz-> 30 40 50 60 70I 80 90 100 110 120 130 140 Abundance #35067: Pyridine, 4-nitro-, 1-oxide (CAS) $$ p-Nitropyridi... 1-0
5000 39 110 ■ i ■ ■ ■ i ■ ■ 1 ■ i 1 ■ 1 1 i ' 51 13.00 13.20 13.40 13.60 13.80 45 63 124 m/z 70.10 12.50% 84 94 - .■I1............. — ----- | Of miz-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35063: 2-Hydroxy-5-nitropyridine $$ 5-Nitro-2-hydroxypyri... 1-0 ■ i ■ ■ 11" , r i-rm-p- 13.00 13.20 13.40 13.60 13.80 5000 m/z 94.00 10.28% 66
80 93 110 0 ........... 49...... , 1..... 1.... 1 1 -.. -H -F — 124 I • ■ i ■ ■ ■ ■ i 1 ' ‘ ■ i ' ■ ‘ ‘ i ‘ 1 ’I m/z— > 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35124: 2,5-Cyclohexadiene-1,4-dione, 2,5-dihydroxy- _ 4 ------ 1-0 13.00 13.20 13.40 13.60 13.80 42 69 m/z 141.00 8.95%
5000 53 84 112
0 ’'J•*’* I | 1 I11-1**111/////11/2/8/1/1/23 ‘ f I ‘ ‘ ‘ ‘ I ' 1 1 111 1 ■ i 1 "II ' ■' i ■ ■ ■ ■ i • ■ m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 13.00 13.20 13.40 13.60 13.80
03514.D HP022102.M Fri Mar 15 10:09:24 2002 Page 14
NYC-WTC_000037757
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NYC-WTC_000037635
Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037760
Laboratory report documenting GCMS analysis of a method blank for sample AE03615 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037720
Laboratory report documenting GCMS analysis of a method blank for sample AE03612 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037780
Gas chromatography-mass spectrometry analysis of sample AE03616 performed on 3/28/2002, detecting other unknown compounds with surrogate 2,4-DDD at 5.0 µg detection limit.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037660
Laboratory report documenting GCMS analysis of a method blank for sample AE03509 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037800
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03617 conducted on March 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037680
Laboratory report documenting GCMS analysis of a method blank for sample AE03510 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037700
Laboratory report documenting GCMS analysis of a method blank for sample AE03611 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009966
Analytical results for sample AE01508 analyzed via GCMS on March 4, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010106
GCMS laboratory results for sample AE01637 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010887
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010967
Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.
1 shared topics · similarity 0.997
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Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
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