Laboratory report documenting GCMS analysis of a method blank for sample AE03614 to verify analytical system cleanliness.
NYC-WTC_000037740–000037759Folder label: “GCMS X 2/19/02 A 3/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02MAR08\03614.D Vial: 4 Acq On : 8 Mar 2002 6:03 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
22.28 0.11 ug/L 88325 Phenanthrene-dl0 22.63
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H12O3 019169-94-9 72 2 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5/53 3 N-perdeuteriobenzy1ideneaniline 192 C13D11N 000538-51-2 53 4 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0 46 Abundance Scan 1675 (22.283 min): 03514. D (-) m/z 192.00 100.00% 192
5000
- 96 146 160 44 54 118 70 82 22.00 22.20 22.40 22.60 O' mPm — TH I “ ’ ‘ I “ * ‘ t mTH m/z 191.00 20.26% m/z—> 20 30 40 50 60 70 80 90 100 11 120 130 140 150 160 170 180 190 200 Abundance #102588: 4-METHOXY-BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192
108 5000 22.00 22.20 22.40 22.60 146 175 m/z 193.00 14.53%
m/z—> 0- ■" i' • ■ ■ i ■ ■" i “1 ‘ i ■ ’ “ i1 ■1 ■ 11 ■ “ i" “ i “ • TUTDTEI[ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 11—111111111’ Ha I Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192 • ■ i • ■ ■ ■ i ■ — 22.00 22.20 22.40 22.60 5000 m/z 146.00 14.51%
96 ........................881 139 152 165 176 . o . 11«j ।. ।. ।»।.»j»।»• p»»ITT «11. । J11 n»।। TITpgut Tur mtz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline / ’ ‘ H ‘ 1 1 I TTEETETEEEr 192 22.00 22.20 22.40 22.60 m/z 96.00 14.04%
5000 82
54 110
m/z—> O 30 ■i “ “i ‘ 111117/111111 94 160 -MH mpnpmpmpmmmmp 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 I T 22.00 22.20 22.40 22.60 11.8
03514.D HP022102.M Fri Mar 15 10:09:24 2002 Page 15
NYC-WTC_000037758
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NYC-WTC_000037635
Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037760
Laboratory report documenting GCMS analysis of a method blank for sample AE03615 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037720
Laboratory report documenting GCMS analysis of a method blank for sample AE03612 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037780
Gas chromatography-mass spectrometry analysis of sample AE03616 performed on 3/28/2002, detecting other unknown compounds with surrogate 2,4-DDD at 5.0 µg detection limit.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037660
Laboratory report documenting GCMS analysis of a method blank for sample AE03509 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037800
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03617 conducted on March 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037680
Laboratory report documenting GCMS analysis of a method blank for sample AE03510 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037700
Laboratory report documenting GCMS analysis of a method blank for sample AE03611 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009966
Analytical results for sample AE01508 analyzed via GCMS on March 4, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010106
GCMS laboratory results for sample AE01637 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010887
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010967
Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.
1 shared topics · similarity 0.997
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Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
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