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GCMS analysis results for sample AE00366, Jan 18 2002

Machine-extracted title · confidence 100%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00366 conducted on January 18, 2002.

NYC-WTC_000051236–000051251

Folder label: “GCMS X 1/8/02 A 1/10/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02JAN10\00465.D Vial: 3 Acq On : 10 Jan 2002 4:28 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.13 ug/L 70443 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 64 3 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 59 4 N-(2-methylprop-2-enyl)-2-nitrob. .. 192 C10H12N2O2 000000-00-0 49 Abundance Scan 1656 (22.280 min): 00465. D (-) m/z 192.10 100.00% 19 2

5000

96 ■ i ■ ■ ■ ' i ■

m/z-> 0 RR

....... 1?....,, ..... 1, ^ .., 82 120 ...I'" _10_ TTT 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60 m/z 191.10 h 17.96% Abundance #102588: 4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 5000 22.00 22.20 22.40 22.60 146 175 m/ z 193.10 17.03% 0 +1 TTT m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192

22.00 22.20 22.40 22.60 5000 82 m/ z 96.00 16.26% 54 110 30 1 94 160 0 — TT I" ' ’ I mH mmm TTIT m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192 22.00 22.20 22.40 22.60 m/z 146.10 14.20% 5000

96 165 88 J 139 152 ,| 176 , A 0 " i " " r " ' r " ■ i" " r " 11" d 11111111 " I " " I " 111" "'I" " 11" 11111111" 11 rm" I ‘ II m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 2240 22.60

)0465.D SCAN508.M Fri Jan 11 10:08:30 2002 Page 10

NYC-WTC_000051249

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NYC-WTC_000051249Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.997

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