GCMS analysis results for sample AE00366, Jan 18 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\O2JAN10\00465.D Vial: 3 Acq On : 10 Jan 2002 4:28 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 7 2-Propanol, 1-(2-methoxypro... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 9.84 0.32 ug/L 102790 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxypropoxy) .. . 148 C7H16O3 013429-07-7 83 2 Butane, 2-methoxy- (CAS) $$ Meth... 88 C5H120 006795-87-5 64 3 PROPYLENE GLYCOL TRIMER 1 174 C9H18O3 000000-00-0 43 4 Butane, 2-methoxy- $$ Ether, sec... 88 C5H120 006795-87-5 43 Abundance Scan 566 (9.836 min): 00465.D (-) m/z 59.05 100.00% 59

5000

45 73 104 9.40 9.60 9.80 10.00 10.20 0- ---------- m/z 45.10 13.07% Tl/Z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #43942:2-Propanol, 1-(2-methoxypropoxy)- $$ 1-(2-Methoxyp... 59

5000 M 9.40 9.60 9.80 10.00 10.20 m/ Z 43.10 11.49% 31 45 130 n/z-> 0—1PT 10 20 30 40 50 nlnoii’l,.... loss 73 60 ■ i1 ■ ■ ■ i ■ ■ 1 ■ r ' ■ ■ i 11 ■ ■ i ■ • ■ ■ i ' ■ ■ ■ i ■

70 80 90 100 110 120 130 Abundance #4937: Butane, 2-methoxy- (CAS) $$ Methyl sec-butyl ether... 59 9.40 9.60 9.80 10.00 10.20 5000 m/z 73.10 9.82%

15 27 45 73 0^ . ,,83. 1 ■ l ■ ■ ....... ।.... ......... ......... . . m/z-> Abundance 10 20 30 40 50 60 70 80 90 100 110 120 130 #78532: PROPYLENE GLYCOL TRIMER 1 59 ....... M...... 9.40 9.60 9.80 10.00 10.20 m/z 41.10 9.81%

5000 41 103

73 — 87 117 130 n/z-> 0 .. ।.... । ■ . ■. । . 10 20 30 40 50 1 II 60 ....... 70 80 ■ । 90 ■1 ■ । ■ T' 1 • » | * 1 100 110 | 120 ‘ ( 130 < i ■ ' ■ ■ i 1 1 1 1 1 1 ' 1 1 I ' 9.40 9.60 9.80 10.00 10.20 T

30465 .D SCAN508.M Fri Jan 11 10:08:30 2002 Page 9

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