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GCMS results for sample AE00463, Jan 24 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00463 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051422–000051438

Folder label: “GCMS X 1/8/02 A 1/11/02

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Scanned page image, NYC-WTC_000051434
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN11\00463.D Vial: 5 Acq On : 11 Jan 2002 5:25 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 7 2-Propanol, 1-(2-methoxypro. . . Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 9.85 0.21 ug/L 64052 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxypropoxy)... 148 C7H1603 013429-07-7 78 2 PROPYLENE GLYCOL TRIMER 1 174 C9H18O3 000000-00-0 9 3 .beta.-Fluoroallyl ethyl ether 104 C5H9FO 000000-00-0 7 4 Butanoic acid, 2-hydroxy- $$ But... 104 C4H8O3 000565-70-8 5 Abundance Scan 567 (9.847 min): 00463.0 (-) m/z 59.10 100.00% 59

5000

.... .......................................... ) , 45 73 104 9.60 9.80 10.00 10.20 86 0 — TinT ■ • । ■ i ■ ....g m/z 45.10 11.79% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #43942: 2-Propanol, 1 -(2-methoxypropoxy)- $$ 1-(2-Methoxyp... 59

................ . 5000 9.60 9.80 10.00 10.20 m/z 43.00 9.68% 31 45 73 104 0-T --l- I...................... ,3................. 130 ' i 1 ' ■ ' i ' ■ ■ ' i 1 ' ' 1 i ' 1 ' 1 i ■ ' ' ■ i ' ' ■ ■ i ' lz--> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #78532: PROPYLENE GLYCOL TRIMER 1 59

9.60 9.80 10.00 10.20 5000 41 m/z 41.10 9.39% 103

|-73 87 A 117 130 0 —Tmm ■ ' l 1 TIBUBIBUTTT 1 • ■ i ■ > ■ ■ ■ i ■ ■ • ■ । । mlz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #10165: .beta.-Fluoroallyl ethyl ether 59 -.. - —4.,. 9.60 9.80 10.00 10.20 m/z 58.10 9.35% 5000 45 76 27 33 O' i ■ ■ ■ ■ 1 1 ' i ' — L < > i ■ > ......... 89.......... 104................................ m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 9.60 9.80 10.00 10.20

00463.D SCANSOB.M Mon Jan 14 10:46:57 2002 Page 9

NYC-WTC_000051434

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NYC-WTC_000051434Source: NYC Law Department, mirrored locally

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