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GCMS results for sample AE00314, Jan 24 2002

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Laboratory report showing GCMS analysis of sample AE00314 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051364–000051379

Folder label: “GCMS X 1/8/02 A 1/11/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN14\00314.D Vial: 3 Acq On : 14 Jan 2002 12:09 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 14, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 7 2-Propanol, 1-(2-methoxypro... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 9.85 0.14 ug/L 50621 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxypropoxy)... 148 C7H1603 013429-07-7 74 2 Butanoic acid, 2-hydroxy- $$ But... 104 C4H803 000565-70-8 9 3 PROPYLENE GLYCOL TRIMER 1 174 C9H18O3 000000-00-0 9 4 Formamide, N-methyl- (CAS) $$ N-... 59 C2H5NO 000123-39-7 4 Abundance Scan 567 (9.847 min): 00314.0 (-) m/z 59.10 100.00% 59

5000

0 ■ । ■ ' ■ ■ । ■ i 1 ' 45

। ■ 1 । ' 73 . ............ I............. 104 m/z MJ9.60 45.10 9.80 10.00 10.20 16.09% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #43942:2-Propanol, 1-(2-methoxypropoxy)- $$ 1-(2-Methoxyp... 59

5000 9.60 9.80 10.00 10.20 m/z 73.00 11.98% 31 45 73 104 1 -- 1 1 1 1 1 1 I 1 1 1 1 1 1 1 ■ ' i ' 1 ■ ■ i ■ ' ' ■ i ' ’ ■ 130 1,74 0 Till ' i ■ ■ n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #10063: Butanoic acid, 2-hydroxy- $$ Butyric acid, 2-hydro... 31 59 _AAA 960 9.80 10.00 10.20 5000 m/z 41.10 10.88% 45 .............. 104............................. 0 1 i 1 1 Pr -i । । I Ih'i । । । 111 । n/z-> 20 30 40 50 60 90 100 110 120 130 Abundance #78532: PROPYLENE GLYCOL TRIMER 1 ■ ■ ■ ■ । ■ ■ ■ ■ । 59 9.60 9.80 10.00 10.20 m/z 43.10 10.70%

5000 41 A 103

73 87 ........... 117 130 0 ... 1)1..... n.i. ----- ■ i ■ ■ i ■ IT ‘ I‘* n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 9.60 9.80 10.00 10.20

00314.D SCAN508.M Tue Jan 15 08:47:51 2002 Page 9

NYC-WTC_000051376

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NYC-WTC_000051376Source: NYC Law Department, mirrored locally

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