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GCMS analysis results for sample AE00366, Jan 18 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00366 conducted on January 18, 2002.

NYC-WTC_000051236–000051251

Folder label: “GCMS X 1/8/02 A 1/10/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN10\00465.D Vial: 3 Acq On : 10 Jan 2002 4:28 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 5 2-Propanol, 1-(2-methoxy-l-... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 9.54 0.15 ug/L 49021 1,4 -Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methy... 148 C7H1603 020324-32-7 83 2 2-Propanol, 1,1'-oxybis- (CAS) $... 134 C6H14O3 000110-98-5 39 3 2-Propanol, 1,1'-oxybis- (CAS) $... 134 C6H14O3 000110-98-5 39 4 2-Butanol, 3,3'-oxybis- 162 C8H18O3 054305-61-2 9 Abundance Scan 540 (9,539 min): 00465.D (-) m/z 59.10 100.00% 59

5000 45 103 73 1 9.20 9.40 9.60 9.80 0 1 1 1 ' 1 1 i ' 1 — ' i ■ ■ ■ ■ i ■ ■ ' ■ i ■ ■ 1 1 i ■ ■ ■ • i ■ m/z 45.10 42.10% z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #43943: 2-Propanol, 1 -(2-methoxy-1 -methylethoxy)- $$ Dipro... 59

5000 45 73 103 ... M., 9.20 9.40 9.60 9.80 31 m/z 103.10 33.23% 0 'i 1 1 1 1 i 1,1 ' 1 । । ' । TIT —1 I" " r ..................... .. t -’I ■ ■ i ' ■ ■ ' i b ■ ' 130 ■ I ■ ■

m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #29204: 2-Propanol, 1,1-oxybis- (CAS) $$ Dipropylene glyc... 59 1 b

9.20 i 1 ■ • ■

9.40 i ■ 1 A 9.60 9.80 31 m/z 73.10 25.88% 5000 45 103

0 ■ i > ■ ■ ■ i ■ • 1 • i ------------------ m/z-> Abundance 20 30 40 50 60 70 80 90 100 110 120 130 #29205:2-Propanol, 1,1 '-oxybis- (CAS) $$ Dipropylene glyc... 59 ..... WMM. 9.20 9.40 9.60 9.80 m/z 41.10, 22.36% 31 5000 45

103

'i ... 0T mlz-> 20 30 40 50 60 70 80 90 100 110 120 130 9.20 9 40 9.60 9.80

0465.D SCAN508.M Fri Jan 11 10:08:29 2002 Page 7

NYC-WTC_000051246

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NYC-WTC_000051246Source: NYC Law Department, mirrored locally

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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