GCMS DFTPP calibration report, Feb 5 2002

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Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB05\00028A.D Vial: 4 ’ Acq On 5 Feb 2002 5:27 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 2-Propanol, 1-(2-methoxy-l-... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 9.54 0.15 ug/L 106955 1,4-Dichlorobenzene-d4 9.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methy... 148 C7H16O3 020324-32-7 83 2 2-Propanol, l,l'-oxybis- (CAS) $... 134 C6H1403 000110-98-5 72 3 BIS(1-METHYL-2-HYDROXYETHYL)ETHER 134 C6H1403 000000-00-0 56 4 2-Butanol, 3,3'-oxybis- 162 C8H18O3 054305-61-2 56 Abundance Scan 540 (9.539 min): 00028A.D (-) m/z 59.10 100.00% 59

iz-> 5000

0-PPPTT -P ii 20 30 40 45

50 60 70 73

84 90 103

। ■ i ■ ■ ■ ■ i ■ > - । i ■ ■ ■ ■ । - i ■ ■ i ■ ■ ■ - i । ■ ■ ■ i ■ ■ i > l ■ 80 100 110 120 130 140 9.20 m/ z 9.40 45.10 M 9.60 9.80 41.68% Abundance #43943: 2-Propanol, 1 -(2-methoxy-1 -methylethoxy)- $$ Dipro...

MA 59

A 5000' 45 103 9.20 9.40 9.60 9.80 73

_M 31 m/z 103.10 36.29% 1HI.. 130 0- TT' ' 1 1 I1 1 1 1 1 1 . .......... . " rr Pr niz-> 20 30 40 50 (60 70 80 90 100 110 120 130 140 Abundance #29198:2-Propanol, 1,1‘-oxybis- (CAS) $$ Dipropylene glyc... 59

31 9.20 9.40 9.60 9.80 5000 45 m/z 73.10 27.18% 103 89 0- 'i■■'' I' ' ' ■ i 1 1 i ■ ' 1 'H1’' ■ ■ 72 - m/z~> Abundance 20 30 40 50 (60 70 80 90 100 110 120 130 140 #29208: BIS(1-METHYL-2-HYDROXYETHYL)ETHER 50 __ NW.A 9.20 9.40 9.60 9.80 m/z 41.10 22.23% 5000 31 45 103

0- % •11#'T1 ■ ■ ■ i ■ ■ '■i1■■■i■■ ' ■ i ' 1 • ■ i '' 1 ' i 1 '■‘i134 ■1■ ' i ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ' ■ i ■1 11 f । > 11 m/z-> 20 30 40 50 (60 70 80 90 100 110 120 130 140 9.20 9.40 9.60 9.80

00028A.D HP020702.M Thu Feb 21 15:48:53 2002 Page 7

NYC-WTC_000004850

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