GCMS DFTPP calibration report, Feb 5 2002

Machine-extracted title · confidence 95%

Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB05\00028A.D Vial : 4 Acq On 5 Feb 2002 5:27 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 2-Propanol, 1-(2-methoxy-l-... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T.

9.63 0.16 ug/L 119950 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-l-methy... 148 C7H1603 020324-32-7 72 2 BIS(1-METHYL-2 -HYDROXYETHYL)ETHER 134 C6H14O3 000000-00-0 64 3 2-Butanol, 3,3’-oxybis- 162 C8H18O3 054305-61-2 64 4 E-Dipropylene glycol $$ 2-hydrox... 134 C6H14O3 000000-00-0 59 Abundance Scan 548 (9.630 min): 00028A.D (-) m/ z 59.10 100.00%

_M 59

5000 45 103 73 —— 86.............. |j..................................... 9.20 9.40 9.60 9.80 10.00 O' I 1 ' 1 1 1 1 1 m/z 45.10 43.64% m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #43943:2-Propanol, 1-(2-methoxy-1-methylethoxy)- $$ Dipro... 59

5000

31 45 73 103 9,20 9.40 m/z 103.05i 9.60 LN , ' ' 9.80 10.00 39.48% 130 0 ■i ■ ' 1 1 I' ■ ■ ■ i 111 I-P--t .................. ......... ।. 11111 i ' ' 1 ■ i ■ ■ ■ 1 i ' ■ ' ■ i ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #29208: BIS(1-METHYL-2-HYDROXYETHYL)ETHER 59 i ■ ■ ■ ■ i ■ ■ 9.20 9.40 9.60 AMA— 9.80 10.00 5000 31 m/z 73.10 25.42% 45 103

-4 TT4 134 miz-> 0 ■ i ■‘ 1 1 i ' '

Abundance 20 30 40 50 I' ■ ■ ■ i ■ 1 ' ■ i 1 ' ■ ■ i ■ ■ ' ■ i ' 1 ■ ' i ' ■ ■ ■ i ■ ■ ■ ■ i ■ ' 1 ■ i ■

(60 70 80 #61826:2-Butanol, 3,3’-oxybis- 59 90 100 110 120 130 140 _ NA 9.20 9.40 9.60 9.80 10.00 m/z 41.10 22.86%

5000 31 45 103

O' । ■ ■ " i ■■ —ri 11 'i111,1 I'1 ■ 1 1 i ' ■ ■ ■ i 1 1 ' ' i 1 ■ ■ ■ i ■ 1 ■ ■ i ■ 1 ■ ■ i 1 ' ■ ' i 134 ■ ■ ' ■ i ' mfz-> 20 30 40 50 (60 70 80 90 100 110 120 130 140 9.20 9.40 9.60 9.80 10.00

00028A.D HP020702.M Thu Feb 21 15:48:53 2002 Page 8

NYC-WTC_000004851

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