GCMS DFTPP calibration report, Feb 5 2002

Machine-extracted title · confidence 95%

Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

Page image

OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB05\00028A.D Vial: 4 Acq On 5 Feb 2002 5:27 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 Acetic acid, 3-[1,3]dioxola... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 5.92 0.21 ug/L 157009 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 28 2 3-(CYCLOHEX-3 ’-EN-YL)PROPANOL $$.. . 174 C8H14O4 015745-87-6 28 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 Pentanol, 5-amino-_________________ 103 C5H13NO 002508-29-4 9 Abundance Scan 223 (5.920 min): 00028A.D (-) m/ z 73.10 100.00% 73

5000 43 ' I ' ' ' ' I 5.60 5.80 6.20 m/z-> o1 In-. 7.... 1111753, '.. .............................. . 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 m/ z 43.10 25.21% Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 —A— ■ i ■ ■ ■ ■ i 5.60 5.80 6.00 6.20 43 m/ z 41.10 10.16% 27 55 87 113 174 0- ppm 11" " I " ' 'T' r TNTpmmg TTTn] ,i

miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 0.. , 1. 1 ■ i ' ■ ■ 1 i 5.60 5.80 6.00 6.20 5000 m/ z 45.10 9.32% 43 27 87 0- TTTT 11"55" 11" 'T' , i TTT 174 113 I''1" I i. ■ ■. i i ■1" i ■"' । ■11' i ■ miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... AI 30 5.60 5.80 6.00 6.20 73 m/z 74.10 6.08% 5000 44 58

15 - 0- i'l " -T i' । ■ ■ i1 ■ ■ ■ i' • ■ ■ i " ■ ■ i ■ ■111 ■ ■ ■ 111 ■ ■ ■ i ■'1 ■ i ■ ■ ■, i • ■ ■ ■ ।'' ■, i ■ ■ ■ i ........... ■ i 1 । । 1 I । 1 । । I m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

00028A.D HP020702.M Thu Feb 21 15:48:53 2002 Page 6

NYC-WTC_000004849

OCR can misread numbers and units. Confirm readings against the page image before using them.

NYC-WTC_000004849Source: NYC Law Department, mirrored locally

Related records

Browse subjects →

Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.

Same-box records

DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998