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GCMS analysis results for sample AE00366, Jan 18 2002

Machine-extracted title · confidence 100%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00366 conducted on January 18, 2002.

NYC-WTC_000051236–000051251

Folder label: “GCMS X 1/8/02 A 1/10/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN10\00465.D Vial: 3 Acq On 10 Jan 2002 4:28 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 2-Propanol, 1-(2-methoxy-1-... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

9.63 0.18 ug/L 57892 1,4-Dichlorobenzene-d4 9.72

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methy. . . 148 C7H16O3 020324-32-7 64 2 4-(Dimethylamino)-1,3-diazaspiro... 209 C11H19N3O 000000-00-0 45 3 TRIPROPYLENE GLYCOL 2 192 C9H20O4 000000-00-0 45 4 TRIPROPYLENE GLYCOL 1 192 C9H20O4 000000-00-0 45 Abundance Scan 548 (9.630 min): 00465.D (-) m/z 59.05 100.00% 59

5000

0- JU 45 73

I •11 • I 86 T 103

r i " " i " " r • " r " ■ i1'' ■ r 1" 11 ■ " i" " i " i 9.20 9.40 m/z 103.10 V 9 60 > ■ i • ■ > • i 9.80 10.00 46.91% m/z--> 30 40 50 60 70 80 90 100110120130140150160 170180190200 210 Abundance #43943: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- $$ Dipro... 59

5000 45 73 103 i ■ • > ■ i ■ • 9.20 9.40 9.60 A 9.80 1000 31 m/z 45.10 44.92%

n/z-> 0 --Br m 130 1"11"UTB"TTETTTTTTT"T"TTFI ‘ ‘ 30 40 50 60 70 80 90 100110120130140150160 170180190200 210 T.‘‘ I T

...... N... Abundance #128682:4-(Dimethylamino)-1,3-diazaspiro[4,6]undec-3-en-2-on 50 45 9.20 9.40 9.60 9 80 10.00 5000 m/z 73.10 28.36% 73 N 103 0 | 209 T’’T’011’0ICCIOUTTTTTTTTTTTTT i" "i m/z-> Abundance 30 40 50 60 70 80 90 100110120130140150160 170180190200 210

59 #102327: TRIPROPYLENE GLYCOL 2 9.20 AL9.40 9.60 9.80 10.00 m/z 41.10 19.57%

m/z-> 5000

0 45

-—72.—.89. 103 , 117 130 30 40 50 60 70 80 90 100110120130140150160 170180190200 210 161 i" " i" " i * ■H l 9.20 9.40 W 9 60 9.80 10.00

10465.D SCAN508.M Fri Jan 11 10:08:29 2002 Page 8

NYC-WTC_000051247

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NYC-WTC_000051247Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.997

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