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GCMS analysis results for sample AE00830, Feb 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00830 including surrogate recovery and unknown compounds.

NYC-WTC_000052047–000052068

Folder label: “GCMS X 1/11/02 A 1/31/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN31\00830.D Vial: 3 Acq On : 31 Jan 2002 12:11 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 7 2-Propanol, 1-(2-methoxy-1-.. Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 9.58 0.07 ug/L 34118 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methy... 148 C7H16O3 020324-32-7 40 2 4-(Dimethylamino)-1,3-diazaspiro... 209 C11H19N3O 000000-00-0 9 3 2-Butanol, 3,3'-oxybis- 162 C8H18O3 054305-61-2 9 4 2-Propanol, l,l'-oxybis- (CAS) $... 134 C6H1403 000110-98-5 9 Abundance Scan 544 (9.584 min): 00830. D (-) m/z 59.10 100.00% 59

121

5000 45 79 103 .....M,.. 9 20 9.40 9.60 9.80 10.00 0 i" " i ’1" r ■ " i ■1" r ■11 r "' i ■ " ’ I" " i" " i" " i" " i" " i"'11 i1 ■1 ■ i ’ " m/z 121.10 67.15% m/z-> :20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance! #43943: 2-Propanol, 1 -(2-methoxy-1 -methylethoxy)- $$ Dipro... 59

5000 45 103 9.20 9.40 9.60 9.80 10.00 73 31 m/z 45.10 43.40% 0 T ‘ i" " i" " r।1" i" " i'11130 ■ I" " i" " i"1' I" " r ‘" i" " i" " i'"11" " I n/z-> :20 30 40 50 60 70 80 90 100110120130140150160170180190200 210 Abundances #128682:4-(Dimethylamino)-1,3-diazaspiro[4,6]undec-3-en-2-on 59

45 9.20 9,40 9.60 9.80 10.00 5000 m/ z 41.10 37.32% 73 103 209 0- ' i" " i" " i " ‘ ।1'1 ■ i ■" ‘ i1" 1 r'" i" "| i" " i" “ i" " i" " i" " i" " i" " i'1" I " " i"1' r "11" " i m/z-> Abundance: :20 30 40 50 60 70 80 90 100110120130140150160170180190200 210

59 #61826: 2-Butanol, 3,3’-oxybis- 9.20 M 9.40 9.60 9.80 10.00 m/z 103.00 31.56%

5000 31 45 103 N

m/z-> 0 H —p l •" i" ■ • i" " r ■1' i' 134 20 30 40 50 60 70 80 90 100110120130140150160170180190200 210 1 r>111!‘‘1 9.20 9.40 1"ir 9.60 9.80 10.00

00830.D SCAN508.M Fri Feb 01 09:18:32 2002 Page 9

NYC-WTC_000052059

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NYC-WTC_000052059Source: NYC Law Department, mirrored locally

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