GCMS analysis results for sample AE00830, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\5973N\02JAN31\00830.D Vial: 3 Acq On : 31 Jan 2002 12:11 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 8 2-Propanol, 1-(2-methoxypro... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 9.88 0.11 ug/L 49331 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxypropoxy)... 148 C7H16O3 013429-07-7 9 2 Guanidine $$ Aminoformamidine $$... 59 CH5N3 000113-00-8 4 3 Propanoic acid, 2-hydroxy-2-meth... 104 C4H803 000594-61-6 4 4 6-Methoxy-4-oxa-heptanal $$ Prop... 146 C7H14O3 089769-34-6 4 Abundance Scan 570 (9.881 min): 00830.D (-) m/z 59.10 100.00% 59

5000

‘I’*

/z-> 0-T 20 1 45 ' I 1 b If I 'I" ‘I’’ 30 40 50 60 70 80 90 100 110 120 130 9.60 9.80 10.00 10.20 m/z 45.10 15.82% Abundance #43942: 2-Propanol, 1-(2-methoxypropoxy)- $$ 1-(2-Methoxyp... 59

5000 9.60 9.80 10.00 10.20 m/ z 41.10 10.94% 31 45 O—TT -A' ... 'ill... ' I 73 .....' 1 I104' 1 ' .... 1 ' ‘ ’ I ' ' rr I ‘ 130 ' I ' ' ' » | FTT . | . I /z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #621: Guanidine $$ Aminoformamidine $$ Aminomethanamidine ... 43 59 IiT __ 9.60 9.80 10.00 10.20 5000 m/ z 73.00 10.68%

27 ... 01 ' i II r , ■ , ■ , ■ ,i| > + tt+ ITT ■ i ■ 1 ■ ’ i ■ 1 ‘ I‘ 1 ■ ' ■ । । । . m/z--> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #10065: Propanoic acid, 2-hydroxy-2-methyl- $$ Lactic acid... Ar \ ; ' ' I 1 ' ' 1 I ' .... jvi 59 9.80 10.00 10.20 9.60 m/z 104.10) 10.25% 43 31 5000

m/z--> 0 ... I I, ■ i ■ ■ ■ ■ I' 20 30 37+ 40 50 (60 111 - < ■ । 70 * 11 80 86 •1 ■ ■ । ■ ■ ■ ■ । ■ ■ ■ • । >1 ' ■ । 90 100 110 120 । । 130 < 1r1 1 1 1 i 1 1 Tn-j-t-r-T-r-p-r 9.60 9.80 10.00 10.20

00830.D SCAN508.M Fri Feb 01 09:18:32 2002 Page 10

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