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GCMS results for sample AE00314, Jan 24 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00314 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051364–000051379

Folder label: “GCMS X 1/8/02 A 1/11/02

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Scanned page image, NYC-WTC_000051375
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN14\00314.D Vial: 3 Acq On : 14 Jan 2002 12:09 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 14, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 (S)-2-Methylpentan-3-ol Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

9.57 0.11 ug/L 37950 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 (S)-2-Methylpentan-3-ol 102 C6H140 000000-00-0 9 dQ 6009 2 Butanamide, 3-methyl- (CAS) $$ 1... 101 C5H11NO 000541-46-8 9 o* 3 E-Dipropylene glycol $$ 2-hydrox... 134 C6H14O3 000000-00-0 9 MR 4 PROPYLENE GLYCOL TRIMER 1 174 C9H18O3 000000-00-0 9 Abundance Scan 543 (9.573 min): 00314.D (-) m/z 59.10 100.00% 59

5000

0 . 45 4C

lx 73 84 103 9.20 m/z _M9.40 45.10 9.60 9.80 41.37% 1000 ’ I ' ' ' • I ’ ‘ 1 1 TTil m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #9753: (S)-2-Methylpentan-3-ol 59 73 31 5000 41 9 20 9.40 9.60 9.80 10.00 m/z 41.10 39.30% ..... 11.. 1 I 01 ' ' I ' ' ' ' I ' ' ’ • I ■ " ' ■ I ■ ■ ■ ' I 1 84 i ■ ■ ■ ■ i ■ ' • ' i ' । ' I ' ' ' ' i 1 1 ■ ' i ' n/z-> 10 20 30 40 60 50 70 80 90 100 110 Abundance #8825: Butanamide, 3-methyl- (CAS) $$ Isovaleramide $$ Iso... V 59 ..................... ..........................

920 9.40 9.60 9.80 10.00 5000 m/z 40.00 35.12% 44 29 86 15 ...... J ........ ....... 1 69 100 0 ' i ' ' ' ' i ' ' ■ ■ i ‘ ‘‘I* ■ i ■ • ■ ' i ' — 1 I' ' ' ' I ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #29239: E-Dipropylene glycol $$ 2-hydroxyethyl ether 31 59 9 20 9.40 9.60 9.80 10.00 m/z 43.10 26.69%

5000 45 103 39 . 0 ■UI ill. n . Ill.... ..................... ... • i ■ • • > i ■ ■ TU." TT n/z-> 10 20 30 40 50 60 70 80 90 100 110 9.20 9.40 9.60 9.80 10.00

30314.D SCAN508.M Tue Jan 15 08:47:51 2002 Page 8

NYC-WTC_000051375

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NYC-WTC_000051375Source: NYC Law Department, mirrored locally

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