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GCMS results for sample AE00314, Jan 24 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00314 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051364–000051379

Folder label: “GCMS X 1/8/02 A 1/11/02

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Scanned page image, NYC-WTC_000051374
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN14\00314.D Vial: 3 Acq On : 14 Jan 2002 12:09 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 14, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L Peak Number 5 Acetic acid, 3-[1,3]dioxola... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.89 4.67 ug/L 1655650 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 23-(CYCLOHEX-3‘-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 25 4 Silane, tetramethyl- (CAS) $$ Te... 88 C4H12Si 000075-76-3 9 Abundance Scan 220 (5.885 min): 00314.D (-) m/ z 73.10 100.00% 73 5000 43 5.60 5.80 6.00 6.20 0- himpirv.... 11,11/55,... 1 1... 87... 103 r 1 ■ • I' ‘ * I I • • I I • ■ I ' I I'11' I i ■ • i ■■■•। m/z 43.10 24.77% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-(1,3)dioxolan-2-ylpropyl ester 70

5000 5.60 5.80 6.00 6.20 43 m/z 41.10 9.25% 27 55 113 87 174 0 i • ’ " i " “ i TTr I " ‘ ’ I ■ i ■ ■ " i " ' ‘I‘ ..... 1′1 I i ■ ■ ■' i 1’*’’ n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 70 .0/ r 5.60 5.80 6.00 6.20 5000 m/z 45.10 9.21% 43 27 55 113 87 174 0TT r "' i TT ,I r "■I "'''I ■ i" ■ ■ i" " I ■1 ■ ’ r " ■ i i • ■ ■ ■ i ■ ‘ I'1' ’ I' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4814: Silane, tetramethyl- 70 5.60 5.80 6.00 6.20 m/z 71.10 6.41% 5000

45 15 IBuip’".... . 488 1 53 A , I 0 i''' ■ i i " ■ ■ i ■ " ■ i' " ' r ' ■ ■ i ■ ■ ■ ■ i1 " ■ r ' " i T‘ m/z-> 10 :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5,60 5.80 6.00 6.20

30314.D SCAN508.M Tue Jan 15- 08:47:51 2002 Page 7

NYC-WTC_000051374

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NYC-WTC_000051374Source: NYC Law Department, mirrored locally

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