DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004494–000004704

Folder label: “GCMS X 1/30/02 A 2/26/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB26\02084.D Vial: 1 Acq On : 26 Feb 2002 2:44 pm Operator: Sample : 508 scan Inst Instrumen Mise : February 2 6, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L Peak Number 7 Acetic acid, 3-[1,3]dioxola... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 5.95 0.32 ug/L 142840 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 40 2 3- (CYCLOHEX-3' -EN-YL) PROPANOL $$ . . . 174 C8H14O4 015745-87-6 40 3 Propane, 2-methoxy-2-methyl- (CA... 88 C5H120 001634-04-4 9 4 N,N-DIMETHYL-2-BUTOXYISOPROPYLAMINE 159 C9H21NO 000000-00-0 9 Abundance Scan 228 (5.948 min): 02084.D (-) m/z 73.10 100.00% 73

5000

1 55 ! 5.60 5.80 6.00 6.20 0- ----- i 87 103 TTPWIPTTRTTTTTTTTLPOTLTTTTIPTUIIIIIWTTTIWTIWTL- m/z 43.1.0 23.53% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[ 1,3]dioxolan-2-ylpropyl ester 73

A______ 5000 ■ ' i ' ■ ' 1 i 1 ■ ■ 1 i ' 1 ' ' i ' 1 ' ■ i 1 5.60 5.80 6.00 6.20 43 m/z 45.05 7.46% 27 55 ,i 87 113 174 0 Tp 1r i"11 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 ' ' i ■ ■ 1 ■ i ' ' ' 1 i ■ ' r 1 i ■ ' r ' i 1 5.60 5.80 6.00 6.20 5000 m/z 71.10 6.32% 43 27 55 . 87 113 174 0-TTTTTTTTTT ' i i ‘1 ‘ ‘ i1 +T— TPuu r ■ " i " " r ■ " i' " ■ r ■111'1" r m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4942: Propane, 2-methoxy-2-methyl- (CAS) $$ Methyl tert-b... 70 5.60 5.80 6.00 6.20 m/z 74.00 4.99%

5000 41 57 15 27 0 " i" " i " " i' 111 III 111 ''I' l11 " 11 —pmmnmmmmmmmp m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

02084.D HP0221.02.M Wed Feb 27 08:34:47 2002 Page 9

NYC-WTC_000004597

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NYC-WTC_000004597Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999