GCMS analysis results for sample AE03246, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03246 conducted on March 15, 2002.

NYC-WTC_000006105–000006125

Folder label: “GCMS X 2/12/02 A 3/01/02”

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NYC 9/11 Public Portal Document Library Search Compound Report . Data File : C: \MSDCHEM\1\5973N\02MAR01\03246.D Vial: 1 Acq On : 1 Mar 2002 4:00 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 Acetic acid, 3 -[1,3]dioxola... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 5.89 4.35 ug/L 2100370 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 2 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 3 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 33 4 3-Pentanol, 2,4-dimethyl-___________ 116 C7H160 000600-36-2 33 Abundance Scan 223 (5.891 min): 03246.D (-) m/ z 73.10 100.00% 73

5000

43 1 1 1 i ' ■ ■ ' i 1 1 1 1 i ' ■ ■ ‘

87 103 5.60 5.80 6.00 6.20

m/z-> 0'i । > 11111 20 30 101 55 ... ,, " ' ■ i1 ' i ■ ■'' i 1 ' i1 ■ ■ ■ i' ■'11''1 1 i''1' i'' ■ ‘ i ■ ■ ‘ ■ i1 ''' r

40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 m/z :43.10 23.34% Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 1 1 ■ i 1 1 5.60 5.80 6.00 6.20 43 m/z -45.10 9.12% 27 55 , 87 113 174 0 ' 111''' I " 111'111 1 r ■ ■111 1 ' 'T' TTImunt’’utamm1—umO1—uu—unuumo——tn] m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5.60 5.80 6.00 6.20 5000 m/ z 41.10 9.07% 43 27 55 , 87 113 174 0-- 111' ■ ■ i1'1 • i • lasgsssns-ss’dd-121101214****////// m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #9702: Butane, 2-methoxy-2-methyl- $$ Ether, methyl tert-p... 73 5.60 5.80 6.00 6.20 m/z 71.00 6.26% 5000

55 87 27I 45

m/z-> 1 — TITJTTTTCTIWIWTITITT 0 ' I ■ ■ ■ ■ i " 11 1TT77TT [11 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 -A 5.60 5.80 6.00 6.20

53246.D HP022102.M Mon Mar 04 12:33:14 2002 Page 10

NYC-WTC_000006118

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NYC-WTC_000006118Source: NYC Law Department, mirrored locally

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