DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB26\02088.D Vial: 5 Acq On : 26 Feb 2002 6:06 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 26, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 Acetic acid, 3-[1,3]dioxola... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 5.95 0.38 ug/L 183322 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y.. . 174 C8H14O4 000000-00-0 36 2 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 36 3 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 4 1-Propene-1-thiol 74 C3H6S 000925-89-3 9 Abundance Scan 228 (5.948 min): 02088. D (-) m/z 73.10 100.00% 73

5000 43 1 r । ' 1 ' 1 i • 55 , 87 103 5.60 5.80 6.00 6.20 - 01' 1........ 11 r I ■ ■ > > ।1 ' ' ■ T' TTTUOaTTTT—aU] m/ z 43.10 25.85% nlz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 A -N * 1 1 * 1 1 1' 1 1 ' 1 1 5.60 5.80 6.00 6.20 43 m/ z 45.10 10.59% 27 87 55 113 , 174 0 mpi’...... 'I1' 11 ‘ ■ i ■ >1 ■ T ■ *t,*’’aI’d’II’tt’nddndnstdm*sdAt* n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 5.60 5.80 6.00 6.20 5000 m/z 41.10 10.35% 43 27 55 87 113 174 0-.................. ... . ■ i " 1' i11'' i' । 1 1 [ > > r* ।IIIIIIIIIII*IIIIG| m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #9663: 3-Pentanol, 3-methyl- ' 1 i 1 ' 1 1 i ' 1 73 5.60 5.80 6.00 6.20 m/z 71.10 6.04%

5000 55 45 87 27 _L 0 ■ i ■'1 ,1 1 ■ i1 ■ ■ ■ । ■" ■ । ’ TTT -TTTmmmmmmm] _____ ________________ ______ 1 1 । 1 1 1 ■ । > 1 ■ 1 । * ‘ 1 • । 1 1 * 1 । ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

02088.D HP022102.M Wed Feb 27 08:35:15 2002 Page 9

NYC-WTC_000004637