DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004494–000004704

Folder label: “GCMS X 1/30/02 A 2/26/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02FEB26\02088.D Vial: 5 Acq On : 26 Feb 2002 6:06 pm Operator: Sample : 508 scan Inst : Instrumen Mise 2002 : February 2 6, Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 Butanoic acid, 2-propenyl e... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T.

5.72 0.06 ug/L 27829 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butanoic acid, 2-propenyl ester ... 128 C7H12O2 002051-78-7 9 2 4-METHOXY-2-BUTEN-1-OL $$ 2-Bute... 102 C5H10O2 026089-32-7 9 3 2-Butene, 1,4-dimethoxy- 116 C6H1202 026649-86-5 9 4 2-METHYLBUT-3-EN-2-OL 86 C5H10O 000000-00-0 7 Abundance Scan 208 (5.722 min): 02088. D (-) m/z 43.10 100.00% 43 71

5000 51 AAA 86 5.40 5.60 5.80 6.00 01 ITTTT ' i' “ ■ i ■' ■ ■ i'1 m/z 41.10 87.55% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #24319: Butanoic acid, 2-propenyl ester $$ Butyric acid, a... 43 71

5000 27 —H 5.40 1 1 i 1 1 1 1 i 1 1 5.60 5.80 6.00 TTF

m/z 71.00 76.68% 38 57 N 89 100 m/z-> Of TTHT + hipimejmii '" ।11" ।" " i " '11" " i " " I" r' i " " 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #9336: 4-METHOXY-2-BUTEN-1-OL $$ 2-Buten-1-ol, 4-methoxy- ... 41 71 ——————— 5.40 5,60 5.80 6.00 5000 m/z 69.00 38.04% 31 53 84 0+ " ‘ i " " i" " i 11"' ’ ’’14 HTTT mfz—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #16778: 2-Butene, 1,4-dimethoxy- ..... 1 .11.. ' ' ■ i ' ‘ ‘ i ' ■ ■ '" I > ■ r ■ 1 ■ • • > । 4 71 84 5,40 5.60 5.80 6.00 m/z 45.10 33.22%

5000 55 27

33 m/z—> 0 ' " i " " i' ... 'I" ... . " i " ■r i ‘" 11'1" i " 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 I......... iL ..I. L.. 5.40 5.60 5.80 6.00

02088.D HP022102.M Wed Feb 27 08:35:15 2002 Page 8

NYC-WTC_000004636

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NYC-WTC_000004636Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999