Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
NYC-WTC_000037635–000037654Folder label: “GCMS X 2/19/02 A 3/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C: \MSDCHEM\1\5973N\02MAR08\03508.D Vial: 4 Acq On : 8 Mar 2002 1:07 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Butanoic acid, methyl ester... Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
3.61 0.15 ug/L 72967 1,4-Dichlorobenzene-d4 9.72
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 90 2 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 83 3 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 83 4 Butanoic acid, methyl ester (CAS... 102 C5H10Q2 000623-42-7 83 Abundance Scan 21 (3.611 min): 03508.D (-) w m/z 43.10 100.00% 74
5000 59 87 ■ ■| ' I' "1111111 3.50 3.60 3.70 3.80 3.90 4.00 O T r1‘2-t11T T rp-rrTp-rrT-j- —1 l*‘“I“ I TH m/z 74.00 78.21% mz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #9227: Butanoic acid, methyl ester (CAS) $$ Methyl butyrat... 43 74
5000 ■ ■ i “ ■ i ‘ “ * i ‘ ‘ “i “ i 3.50 3.60 3.70 3.80 3.90 4.00 59 87 m/Z 71.00 60.29% 69 102 01 " I ■''' I' ‘ ‘' I' ■' ‘ I' “' I Hmm TTH +t pt TTpTTp-rrrp-H-rrp-rrrp- miz—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #9216: Butanoic acid, methyl ester (CAS) $$ Methyl butyrat... 40 74 1' i ‘ ■ U... 4.. 3.50 3.60 3.70 3.80 3.90 4.00 5000- m/z 41.10 29.84% 27 59 87 ,33 102 Of TTp-r TTHTp Hmmmmpmm +t I'' “ 11 ‘1111 TIJp]pap miz-> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 #9224: Butanoic acid, methyl ester (CAS) $$ Methyl butyrat... 40 AAA .... AAA 3.50 3.60 3.70 3.80 3.90 4.00 74 m/z 59.00 22.64% 5000 27 59 87 0 '11 ■'1' 11 —3 7 Hmm TU 69 +t Impp TTTg 102 T I' ‘‘ I I miz—> 20 25 3035404550556065 70 75 80 85 90 95 100 105110 3.50 3.60 3.70 3.80 3.90 4.00
03508.D HP022102.M Fri Mar 15 10:08:50 2002 Page 3
NYC-WTC_000037641
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NYC-WTC_000037720
Laboratory report documenting GCMS analysis of a method blank for sample AE03612 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037660
Laboratory report documenting GCMS analysis of a method blank for sample AE03509 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037780
Gas chromatography-mass spectrometry analysis of sample AE03616 performed on 3/28/2002, detecting other unknown compounds with surrogate 2,4-DDD at 5.0 µg detection limit.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037740
Laboratory report documenting GCMS analysis of a method blank for sample AE03614 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037680
Laboratory report documenting GCMS analysis of a method blank for sample AE03510 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037760
Laboratory report documenting GCMS analysis of a method blank for sample AE03615 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037800
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03617 conducted on March 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037700
Laboratory report documenting GCMS analysis of a method blank for sample AE03611 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010967
Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004494
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009966
Analytical results for sample AE01508 analyzed via GCMS on March 4, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010867
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE02713 including surrogate recovery.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000037604
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Laboratory report showing GCMS blank analysis results for volatile organic compounds with detection limits below MDL.
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NYC-WTC_000037655
Laboratory report listing concentrations of volatile organic compounds in sample AE03509 analyzed on March 19, 2002.
Filed in the same folder