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GCMS blank results for sample AE03508, March 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.

NYC-WTC_000037635–000037654

Folder label: “GCMS X 2/19/02 A 3/8/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report . Data File : C: \MSDCHEM\1\5973N\02MAR08\03508 . D Vial: 4 Acq On : 8 Mar 2002 1:07 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 ISOBUTYRALDEHYDE, DIMETHYLA... Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 3.93 0.08 ug/L 37878 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 ISOBUTYRALDEHYDE, DIMETHYLACETAL... 118 C6H14O2 000000-00-0 78 2 Propane, 1,l-dimethoxy-2-methyl-... 118 C6H14O2 041632-89-7 78 3 ISOBUTYRALDEHYDE, DIMETHYLACETAL... 118 C6H14O2 000000-00-0 78 4 Propane, 1,1-dimethoxy-2-methyl- 118 C6H14O2 041632-89-7 64 Abundance Scan 49 (3.927 min): 03508.D (-) m/z 75.00 100.00% 75

5000 87 55 41 47 I' 1 ' ' I ' 1 ' ' I S 51 71 84 3.60 3.80 4.00 4.20 miz-> Of Tuu1unp—mu—8f —p -—H -I 5 10 15 20253035404550556065 70 75 808580 95 m/z 87.00 36.01% Abundance #17848: ISOBUTYRALDEHYDE, DIMETHYLACETAL $$ 1 1-Dimethoxyi... 75

5000 87 3.60 3.80 .... L i 1 ■ > । i <' ' 1 । 4.00 4.20 15 55 m/z 55.10 29.65% 27 31 47 59 71 0b “ i" TIOp—n—adanaaaannam “ i “ -HT HT HIPg miz-> 5 10 15 20_25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #17844: Propane, 1,1-dimethoxy-2-methyl-$$ Isobutylaldehy... 75 3.60 1 ' I ' 1 3.80 AAALL 4.20 4.00 5000 m/ z 47.00 17.65% 87 31 47 55 — 43, 59 71 OfTTTTJTTTT| "1111/111 mH TIOH] Hp *pagm miz—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #17847: ISOBUTYRALDEHYDE, DIMETHYLACETAL$$ 1 1-Dimethoxyi... . . | 1 1 , I j . । . , , , । ■ t 75 3.60 3,80 4.00 4.20 m/z 41.10 14.99% 5000 87 31 47 55

O ! 43, 59 71 TOTTTTT 1111111 i111111,11111, ■, H Bpmngor A A miz—> 5 10 15 202530354045505560 65 70 75 80 85 90 95 3.60 3.80 4.00 4.20

03508.D HP022102.M Fri Mar 15 10:08:50 2002 Page 4

NYC-WTC_000037642

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NYC-WTC_000037642Source: NYC Law Department, mirrored locally

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NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.998

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