GCMS blank results for sample AE03508, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report • Data File : C:\MSDCHEM\l\5973N\02MAR08\03508.D Vial: 4 Acq On : 8 Mar 2002 1:07 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 2,2-Dimethoxybutane Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 4.24 0.15 ug/L 70114 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,2-Dimethoxybutane 118 C6H14O2 003453-99-4 64/ 2 2,2-dimethoxybutane 118 C6H14O2 003453-99-4 64 3 Methanethioamide, N,N-dimethyl- 89 C3H7NS 000758-16-79 4 THIAZOLIDINE $$ Thiazolidine, hy... 89 C3H7NS 014446-47-0 9 Abundance Scan 77 (4.243 min): 03508.D (-) m/z 87.10 100.00% 87 55 43 5000

l • » > • | • ■ • • | • • < • | r-r-r 103 3.80 4.00 4.20 4.40 4.60 miz-> 0! -------49— - T’T 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 m/z 89.10 99.92% Abundance #17888:2,2-Dimethoxybutane 87 55

5000 .... H.... . 45 3.80 4.00 4.20 4.40 4.60 27 40 m/z 55.10 69.48% 92 103 miz-> Of 33 TTHI L + Hmmp 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 Abundance #17889:2,2-dimethoxybutane 87 55 AAAALL 3.804.00 4.20 4.40 4.60 ■ i ■ ■ 1 ' i ' ' ■

5000 m/z 43.00 55.24% 45

01 27 33 Tupr .11j.... j।[ i H 92 103 AAiaaam miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 Abundance #5040: Methanethioamide, N,N-dimethy- 89 3.80 4.00 4.20 4.40 4.60 m/z 41.10 16.53%

5000

74

mfz—> 33 o TTp-rrrp-rn j TTIr Jut 56 ml “ ■ i11 • ■ i' • • ■ i' TIp -mp 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 3.80 4.00 TIr 4.20 4.40 4.60

03508.D HP022102.M Fri Mar 15 10:08:50 2002 Page 5

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