DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004935–000005145

Folder label: “GCMS X 2/1/02 A 2/27/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB27\02455.D Vial: 6 Acq On : 27 Feb 2002 7:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 3 Acetic acid, 3-[1,3]dioxola.. . Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 5.94 0.37 ug/L 179690 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 42 2 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H1404 015745-87-6 42 3 3-Pentanol, 2,4-dimethyl- 116 C7H160 000600-36-2 33 4 3-Pentanol, 2,4-dimethyl-___________ 116 C7H160 000600-36-2 33 Abundance Scan 227 (5.936 min): 02455. D (-) m/ z 73.10 100.00% 73

5000 43 5.60 5.80 6.00 6.20 , 87 103 m/z-> 11111158, 0......... . 1 I ■ ■ 11 i ■ ■ ■ ■ i

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 i ■ i ■ ■ ■ ■ f ■ - ■ 11 ■ ■ । । । ■ i ■ ■ > ■ i ■ ■ ■ ■ i ■ ■ • ■ i ■ m/z 43.10 22.83% Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 N 11111 । i-rf i । 5.60 5.80 6.00 6.20 43 m/z 45.00 9.11% 27 55 , 87 113 174 0 ipuni’j...... ’I1'1' ' I ' ■' ‘ I''''T‘ 111111111 " '111 " 11,r| 1' I'11111111111 " i1 " ' i1" ■ i'' ■ ■ r m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1 -p... 73 5.60 5.80 6.00 6.20 5000 m/z 41.10 8.24% 43 27 55 87 113 174 01TTT TT ■ । ■ > ■ > । ■ ■ ■ ’14 —TT Tu—]*]]eguummmmmT n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #17065: 3-Pentanol, 2,4-dimethyl- IA A , , I ■ ' 1 ■ I TT 73 5.60 5.80 6.00 6.20 m/ z 71.10 5.93% 5000 55

43 27

m/z-> 0 11 ■1 ■li 1111'111 20 30 40 50 + nil,60...70. , 8083 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

02455.D HP022102.M Thu Feb 28 08:47:42 2002 Page 5

NYC-WTC_000005114

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NYC-WTC_000005114Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999