GCMS analysis results for sample AD31585, Jan 28 2002

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Laboratory report showing GCMS analysis of sample AD31585 including unknown compounds and surrogate recovery data.

NYC-WTC_000049902–000049915

Folder label: “GCMS X 1/3/02 A 1/17/02”

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NYC 9/11 Public Portal Document Library Search compound Report

Data File : C: \MSDCHEM\1\5973N\02JAN17\31585.D Vial: 1 Acq On : 17 Jan 2002 2:50 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 Acetic acid, 3-[1,3]dioxola... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.89 4.97 ug/L ' 1356040 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 2 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 32 4 Silane, tetramethyl- $$ Tetramet... 88 C4H12Si 000075-76-3 9 Abundance Scan 220 (5.885 min): 31585.D (-) m/ z 73.10 100.00% 73

5000 43 ‘-I***‘1***I* -n-p-r-r-r- । । 55 . 187 103 5.60 5.80 6.00 6.20 0-—pmmm‘ ' 1 | ■ n l । l . ! . .. . ।. . . . । , . . . ।. . . . । i ।. . . . । i .. . j. m/z 43.10 24.91% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic add, 3-f1,3]dioxolan-2-ylpropyl ester 73

5000 ■ • । * *7*18**II*4* . 5.60 5.80 6.00 6.20 43 m/z 45.10 9.89% 27 55 ., 87 113 174 m/z-> mmpm OA“ i11" i ■ ■" i ■ ■1 . . । . . I'. ] . . . . । . . . . ( .-I . . । . « . . ] . . . . j . . . . । . . . . , . . . . t . > . I । i 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 5.60 5.80 6.00 6.20 5000 m/z 41.10 8.77% 43 55 27 0-DpMppTt 11 ““ i “''i- 'I, . . , . .87 I'. । . .. . ( 113 174 . । . I . , (. . , , । . 11 . | i i , i | , ■ . , । , , .. । . I , , !. m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4814: Silane, tetramethyl- ' ‘ i ■ ‘ ' ■ I 1 1 ' I ' ’11*4* * 73 5.60 5.80 6.00 6.20 m/ z 71.10 6.42% 1 5000

45 15 1 53 88 0-TIuangu TIHmt ■ ■ i ■ ' miz—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

31585.D SCAN508.M Tue Jan 22 08:36:51 2002 Page 6

NYC-WTC_000049911

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GCMS analysis results for sample AD31671, Jan 28 2002 · Box DEP Box 28

NYC-WTC_000050024

Laboratory report showing GCMS analysis of sample AD31671 including unknown compounds and surrogate recovery data.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998