GCMS analysis results for sample AE00473, Jan 18 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN10\00366.D Vial: 2 Acq On 10 Jan 2002 3:39 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 2 Acetic acid, 3-[1,3]dioxola... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.89 4.34 ug/L 1399080 1,4-Dichlorobenzene-d4 9.71

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 23-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 3 Silane, tetramethyl- $$ Tetramet... 88 C4H12Si 000075-76-3 25 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 220 (5.885 min): 00366.D (-) m/ z 73.10 100.00% 73

5000 43 5.60 5.80 6.00 6.20 01 ..............1155, + *uaUTTDT । 87 103 '111111'1 " i ■ 'I1111 I'"'I''"I' "'11 m/z 43.10 25.21% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3)dioxolan-2-ylpropyl ester 73

5000 1 1 1 1 I । it '"I । । । 'Tr,r'Tl 1 ' 1 5.60 5.80 6.00 6.20 43 m/z 45.10 9.35% 27 o1TPTTt 55 , i ■ i' Tp 87 113 TIWBPNTRTIIITr i' " ’ i " " i 174 n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 ________ / I—r ‘‘‘‘‘‘I ‘‘ 5.60 5.80 6.00 6.20 5000 m/ z 41.10 9.24% 43 27 55 87 113 174 0 ' i ■r " i ■ TTI+ I " " i " ' + /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4812: Silane, tetramethyl- $$ Tetramethylsilane $$ (CH3)4... ' ■ i 1 1 ' • i 1 ‘'‘I 1 1 1 1 1 1 1 1 73 5.60 5.80 6.00 6.20 m/z 71.10 6.39% 5000

45 15 31 88 1 55 0 "I 1 > f-l-i-r i j>>- 1 > i | II'1 1 |> i'i'I'i i > I I | I " I " " i " " I " 111" " I"111"11 r 1" i1" ■ r " • i " " i ■ । । । । । o ' । । 'i । 'T ■ ' b ■ i ' 1 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

00366.D SCAN508.M Fri Jan 11 10:08:25 2002 Page 4

NYC-WTC_000051259