GCMS analysis results for sample AE00165, Feb 2002

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Laboratory report listing unknown compounds and surrogate recovery for sample AE00165 analyzed on February 13, 2002.

NYC-WTC_000050664–000050682

Folder label: “GCMS X 1/4/02 A 2/4/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C: \MSDCHEM\1\5973N\02FEB04\00165.D Vial: 4 Acq On : 4 Feb 2002 5:37 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1. . .\SCAN5 08. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 Acetic acid, 3-[1,3]dioxola... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.90 1.59 ug/L 759623 l,4-Dichiorobenzene -d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 2 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ . . . 174 C8H14O4 015745-87-6 33 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 23 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 221 (5.897 min): 00165. D (-) " 73.10 100.00% 73

5000 43 ‘ 1 1 * *[++**}‘* 1,11 ,5.60 5.80 6.00 6.20 55 0- mm 11 87 103 ( . . . . ।. . . . । . . . . । . I . . ! . . ■ I । i 1 . I | 1 . . I | . T‘‘*T . . . .'i'i'I .. । . . l'l ( . . . . । m/ z 43.10 24.16% ■nfe-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 5.60 5.80 6.00 6.20 43 m/z 45.10 9.93% 27 87 1 113 174 0- mppmhe I 55 I" 1 ‘.1I' birpstij।। .'I।।।।।।. 111.. 1. n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 ' I ' ' FTh 5.60' ' 5.80 6.00 6.20 5000 m/z i41.10 8.49%

miz-> Abundance 0- 27 Tp »J 55..... I• .1 43 87 113 > + . f. ।.... ।.... । '’‘* ‘ 1* 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 #4814: Silane, tetramethy- 7)3 174 ।.... ।.... ।.... ।,, >, । ■ i > 11

5.60 m/ z 5.80 71.10 1 11111 A' 1 1 1 1 ' 1 r 6.00 6.20 6.61%

5000-

45 15 , I 53 88 0 T]TTHHTp • • i • • •»i * * “ i ■ •" i ‘‘ j “ * • i * • • • i • • • * i • *' * i ‘ ■ i1 • ■ * i ‘ ....... A • ' i 1 • • ■ ।1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

00165.D SCAN508.M Tue Feb 05 09:47:34 2002 Page 6

NYC-WTC_000050673

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NYC-WTC_000050673Source: NYC Law Department, mirrored locally

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