GCMS analysis results for sample AE00473, Jan 18 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN10\00366.D Vial: 2 Acq On 10 Jan 2002 3:39 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 3 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.13 ug/L 71694 Phenanthrene -dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 72 2 2-CYANOCARBAZOLE $$ 9H-Carbazole... 192 C13H8N2 057955-18-7 72 3 Benzo[l,2-c:3,4-c]bis(isothiazol... 192 C8H4N2S2 074960-05-7 64 4 1-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 083415-88-7 50 Abundance Scan 1656 (22.280 min): 00366.D (-) m/z 192.10 100.00% 192

5000

82 96 146 160 22.00 22.20 22.40 22.60 52 66 118 0 . ........... . . . ।■ i. । . 11 i-h..i I.... ...........I■■ ■ ■ i ■ ■' । ■ ■ ■ ■ । ■ I +r m/z 193.10 15.77% mlz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103424:3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192

5000 22.00 22.20 22.40 22.60 96 164 m/z 96.00 13.79% 138 o TTIPTTTTUTTTTTTITTTT I'''' I --PPPPP ‘ I’’ m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200

. a. a Abundance #103420: 2-CYANOCARBAZOLE $$ 9H-Carbazole-2-carbonitrile (CAS 192 22.00 22.20 22.40 22.60 5000 m/z 146.10 13.70%

96 138 0- ■ ■ i' ■ ■' i1'111 ■1'111 ■ ■11' ■ ■ ■ i ■ ■1' i ■ ■ ■ ■ i ■ ■ ■' i''' ■ i ■ - T-rp-r n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102104: Benzo[1,2-c:3,4-c]bis(isothiazole) $$ Benzo[1,2-c... 192 22.00 22.20 22.40 22.60 m/z 191.00 12.89%

5000 45 148 57 69 121 165

m/z-> 0 ' I' '1 ' I' 1 ‘ I ‘ I 1' 1' I I' | Tp-f I ■ ■ ■ ■ I 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 H TT 22.00 22.20 22.40 22.60

00366.D SCAN508.M Fri Jan 11 10:08:25 2002 Page 5

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