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GCMS analysis results for sample AD31676, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AD31676 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050317–000050333

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN23\31676.D Vial: 1 Acq On : 23 Jan 2002 2:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 6 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.15 ug/L 84060 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Cyanocarbazole $$ 9H-Carbazole. .. 192 C13H8N2 057102-93-9 72 2 2-CYANOCARBAZOLE $$ 9H-Carbazole. .. 192 C13H8N2 057955-18-7 72 3 Benzo[1,2-c:3,4-c]bis(isothiazol ... 192 C8H4N2S2 074960-05-7 64 4 fluorene-9-spiro-cyclopropane 192 C15H12 000000-00-0 53 Abundance Scan 1656 (22.280 min): 31676.D (-) m/z 192.10 100.00% 1512

5000

AO 96 J 1 1 ‘ I ■ ' 1 1 I 1 1 ' 1 I1 1 1 1 I ' 1 1 1 22.00 22.20 22.40 22.60 nz—> 42 0 —mpHpp ....... ........... 66 82 30 40 50 60 70 80 90 1(X) 110 120 130 140 150 160 170 180 190 200 l m/z 96.10 13.77% Abundance

yo #103424:3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitriJe (CAS 1$2

5000 AMa/ 22.00 22.20 22.40 22.60 96 164 m/z 191.10 12.63% 0 ■ ■ i • ■" i ■ ■ ■ ■ i ‘ ■ i111 ■ i ■ ■ ■' i" I,......... Il 221’021000111117TTrr miz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103420:2-CYANOCARBAZOLE $$ 9H-Carbazole-2-carbonitrile (CAS 192 T 22.00 22.20 22.40 22.60 T A 5000 m/z 193.00 12.36%

O' 9 138 144 . . I I . I . . I . I > > I > I I l l . > > > l > > > l 1 > > I > I > > > > l ) > > > I > > > > I > > l l'l > > I l l > > > > I < I I . I I I ) > I ) I I I I I Wtt miz--> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102104: Benzo[1,2-c:3,4-c]bis(isothiazole) $$ Benzo[1,2-c... 19/2 22.00 22.20 2240 22.60 m/z 146.10 12.28%

5000 45 148 57 69 82 96 miz—> 0- | 121 I . i.... i.... ।. i *." I.. 165 ’ 1’1 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 mm ............. A......... 22.00 22.20 22.40 22.60 —

31676.D SCAN508.M Thu Jan 24 09:57:33 2002 Page 8

NYC-WTC_000050328

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NYC-WTC_000050328Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · similarity 0.996

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