GCMS analysis results for sample AD29522, Feb 2002

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GCMS analysis report for sample AD29522 listing unknown compounds and surrogate recovery data from February 8, 2002.

NYC-WTC_000036779–000036797

Folder label: “GCMS X 12/7/01 A 1/2/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02FEB01\29522.D Vial: 4 Acq On : 1 Feb 2002 1:04 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.14 ug/L 98020 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Cyanocarbazole $$ 9H-Carbazole ... 192 C13H8N2 057102-93-9 72 2 2-CYANOCARBAZOLE $$ 9H-Carbazole ... 192 C13H8N2 057955-18-7 72 3 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H12O3 000607-91-0 53 4 1-Cyanocarbazole $$ 9H-Carbazole ... 192 C13H8N2 083415-88-7 50 Abundance Scan 1656 (22.280 min): 29522.D (-) m/z 192.10 100.00% 192

5000

96 146 160 ■ • i • • • ■ I ■ •

70 82 22.00 22.20 22.40 22.60

miz-> 0 42 Tf I'1' ' I — +H 120 TRmTT ’it IITTDH 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 II— m/ Z 146.10 17.96% Abundance #103424: 3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192

5000 A22.00 22.20 22.40 22.60 96 164 m/z 193.10 17.52%

mz—> 0 ■■ i ‘ ■i■" ■i• “■i “ ■■ i• ■ ■ • i ■ ‘ 1 ‘ I “ • ‘ t ‘ ‘ “ I “1 ‘ 1 ‘ ‘ rt 1’1111111113 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 "1’1 Abundance #103420: 2-CYANOCARBAZOLE$$9H-Carbazole-2-carbonitrile (CAS ' 192 ■ ‘ i ■ ' ' ■ i 1 ' ■ i 1 ■ ‘ ■ i 22.00 22.20 22.40 22.60 5000 m/z 96.10 16.55%

96 164 .................................... ... 04 T I ‘“ I ■ ।" “ । • 111117111171017131111117 miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102624:1,3-Benzodioxole, 4-methoxy-6-(2-propeny!)- (CAS)... 1 1 i ■ ■ ■ ' i 1 ■ ' 1 i ' > ' > 1 1 192 22.00 22.20 22.40 22.60 rn/z 191.10 15.09% 5000

91 165

miz—> O' ill 103 - 177 IT > IJ k J l«) 119 131 5 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 T II 147 I i ■ ■ ■' i — 1’1—0011 22.00 22.20 22.40 22.60 1 29522.D SCAN508.M Mon Feb 04 08:41:12 2002 Page 12

NYC-WTC_000036794

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NYC-WTC_000036794Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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