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GCMS analysis results for sample AD29522, Feb 2002

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GCMS analysis report for sample AD29522 listing unknown compounds and surrogate recovery data from February 8, 2002.

NYC-WTC_000036779–000036797

Folder label: “GCMS X 12/7/01 A 1/2/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB01\29522.D Vial: 4 Acq On 1 Feb 2002 1:04 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 Anthracene-D10 Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.24 ug/L 161468 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-D10 188 C14D10 000000-00-0 80 2 Phenanthrene-diO 188 C-14D10 001517-22-2 68 3 Acridine-D9 188 C13D9N 000000-00-0 64 4 1,2-Bis(2-hydroxyphenyl)ethylene... 376 C24H28N2O2 000000-00-0 59 Abundance Scan 1699 (22.771 min): 29522.D (-) m/z 188.10 100.00% its

5000 94 132 146 160 1801 80 22.40 22.60 22.80 23.00 23.20 42 54 66 | . 20.58% 0- -HHH ------- m/z 94.05 miz-> 40 50 60 70 80 90 100 110 120 130 140 ISO 160 170 180 190 Abundance #84498: Anthracene-D10 188

5000 —I T — 22.40 22.60 22.80 23.00 23.20 80 m/z 189.10 12.51% 94 66 160 i

miz-> 0- mmmH m — mH H frrrr 40 50 60 70 -80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84499: Phenanthrene-d10 188

22.40 22.60 22.80 23.00 23.20 5000 m/z 80.10 12.29%

80 94 160 66 .............. 0- —ITTTIT i “ ■ ■ i T miz—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #85255: Acridine-D9 its 22.40 22.60 22.80 23.00 23.20 m/z 187.20 11.61% 5000

93 158 66 80

m/z—> 0J —m m -2, 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ■ i ■ • V....................... • ! ■ *1 ■ । ■ ■ ■11 • 22.40 22.60 22.80 23.00 23.20

29522.D SCAN508.M Mon Feb 04 08:41:12 2002 Page 13

NYC-WTC_000036795

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NYC-WTC_000036795Source: NYC Law Department, mirrored locally

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