GCMS analysis results for sample AD29522, Feb 2002

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GCMS analysis report for sample AD29522 listing unknown compounds and surrogate recovery data from February 8, 2002.

NYC-WTC_000036779–000036797

Folder label: “GCMS X 12/7/01 A 1/2/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report . Data File : C:\MSDCHEM\l\5973N\02FEB01\29522.D Vial: 4 Acq On 1 Feb 2002 1:04 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 13,14-Dichloro-behenamide Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T.

29.50 0.06 ug/L 38889 Chrysene-dl2 30.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 13,14-Dichloro-behenamide 2 meso-3,4-Hexanediol 407 C22H43C12NO 118 C6H1402 000000-00-0 33 022520-39-4 9 (0 3 2-Hydroxy-2,5-dimethyl-hept-6-en... 156 C9H1602 000000-00-0 9 w/*(ot 4 1-Propanamine 59 C3H9N 000107-10-8 7 Abundance Scan 2288 (29.496 min): 29522.D (-) m/z 59.10 100.00% 53

5000<

T I’ELIIIILIIT 4 86 29.20 29.40 29.60 29.80 O-pm _ 1 11‘ ........................................................................................... 2111110019100191TTTTETIEE‘10211011712E— 7231‘1119121110111‘AU1—"E‘0"TSTTLETTTT m/z 72.10 50.14% m/z—> 20 40 60 80 100120140160180200220240260280300320340360380400 Abundance #336254:13,14-Dichloro-behenamide 53

5000 11. । >. . . । ।. ... ।. 29.20 29.40 29.60 29.80 m/z 43.10 21.61% 4 0 • i *' ■ * r IEI—B—gdgTTmO) 407 m/z—> 20 40 60 80 100120140160180200220240260280300320340360380400 Abundance #17881: meso-3,4-Hexanediol 59 ■ ■ । (। ■ ■ ■ ■ ।f । ■ 29.20 29.40 29.60 29.80 5000 m/ z 55.10 13.34% 41

0- L I mmpmmmmmmmmmmmmmmmmmmmmmmmmmmmmmmp m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #55603: 2-Hydroxy-2,5-dimethyl-hept-6-en-3-one —। । i । । . >. । i । । । । < 53 29.20 29.40 29.60 29.80 m/z 41.10 12.94% 5000

41 98 0 ' I * gl, • ‘ * f ’ ‘1 J 1 Tmnpuudm 11 TIUE—" i TTTIT TTT 111 T’TTT i ■ TE0——01008111 ■ ■ । ■ ■ ■ • । ■4 • । ‘ ■ i • • m/z—> 20 40 60 80 100120140160 "30 200 220 240 260 280 300 320 340 360380400 29 20 29.40 29.60 29.80

29522.D SCAN508.M Mon Feb 04 08:41:12 2002 Page 14

NYC-WTC_000036796

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NYC-WTC_000036796Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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