GCMS analysis report for sample AE01507, March 2002

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Analytical results from a gas chromatography-mass spectrometry test conducted on March 4, 2002, identifying volatile organic compounds.

NYC-WTC_000009986–000010007

Folder label: “GCMS X 1/23/02 A 2/21/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report . Data File : C:\MSDCHEM\1\5973N\02FEB21\01508.D Vial: 8 Acq On : 21 Feb 2002 9:01 pm Operator: Sample : 508 scan fb Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 1-Propanamine (CAS) $$ n-Pr... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 5.02 0.07 ug/L 32918 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Propanamine (CAS) $$ n-Propyla... 59 C3H9N 000107-10-8 9 2 3-Hexanol (CAS) $$ Hexan-3-ol $$. . . 102 C6H14O 000623-37-0 9 3 3-Hexanol (CAS) $$ Hexan-3-ol $$... 102 C6H140 000623-37-0 9 4 3-Hexanol (CAS) $$ Hexan-3-ol $$... 102 C6H140 000623-37-0 9 Abundance Scan 146 (5.022 min): 01508.D (-) m/z 59.10 100.00% 59

5000 73 41 0, , A , A JI 49 4.60 4.80 ‘ 5.00 5.20 5.40 niz-> 0+ “।““।““i“■ ■ i■ ■■ • i ■ alinn) i “ “i “ " i “ 11’1001—009100010—3090933033331—1 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 m/z 55.10 70.76% Abundance #654: 1-Propanamine (CAS) $$ n-Propylamine $$ Propylamine... 59

5000 42 TT-r-r-r-r-p-r 4.80 5.00 5.20 5.40 4.60 m/z 73.00 45.82% 51 TTTT 0 * 'i “ “ i “ “ i11 •11 ■ “ ■ i ■ “ 1 “ ‘' I “ “ I " " I ‘H “ I “ “ I “ “ I " ‘' 111' ‘ I' n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 Abundance #9600:3-Hexanol (CAS) $$ Hexan-3-ol $$ C2H5CH(OH)C3H7 $$ ... 50

31 4.60 4.80 5.00 5,20 5.40 5000 73 m/z 41.10 39.88%

44 niz-> 0 “I "“I' rrf mipaspbljam + inuapuadapul 102 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 .।....(....।.... ।.... 111111111.11. > 111

Abundance #9597:3-Hexanol (CAS) $$ Hexan-3-ol $$ C2H5CH(OH)C3H7 $$ ... H AH ■ l. 59 4.60 4.80 5.00 5.20 5.40 m/ z 43.10 22.99% 31 5000 73

miz-> 44 0 -rrp-rrrp- ’ I . ।. ।.... ।.. J | >. 111. >.. 41 TpH 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 ,।।11ji 1111111 > 1111 > 11 100 AMWA 4.60 4.80 5.00 44r 5.20 5.40 ,A

01508.D HP022102.M Mon Feb 25 10:54:57 2002 Page 7

NYC-WTC_000009996

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