GCMS analysis report for sample AE01507, March 2002

NYC 9/11 Public Portal Document Library Search Compound Report , Data File : C:\MSDCHEM\l\5973N\02FEB21\01508 .D Vial: 8 Acq On : 21 Feb 2002 9:01 pm Operator: Sample : 508 scan fb Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 2-Decanol (CAS) $$ 2-Hydrox... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 5.13 0.10 ug/L 46557 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Decanol (CAS) $$ 2-Hydroxydeca... 158 C10H22O 001120-06-5 9 2 2-Nonanol 144 C9H20O 000628-99-9 9 3 n-Hexyl lactate 174 C9H18O3 000000-00-0 9 4 hexan-2-ol______ 102 C6H140 000000-00-0 9 Abundance Scan 156 (5.135 min): 01508.D (-) m/z 45.10 100.00% 45

5000 A 55 69 "480 5.00 5.20 5.40 ■ • i ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ' ।

miz-> 0- 20 4 . , I III 30 40 50 1 * i ■ ‘ 1 • i ■ ■ ■ ■ i ■ ■ • ‘ i ■' 60 70 80I ■ 87

90 100 110 120 130 ■ ■ i ■ ■ ‘ 1 i ■ ■ ■ • i • ■ • ■ i ■ ■ ■' i ' ■ ■' i 1 ‘ 140 m/z 44.00 23.44% Abundance #58238: 2-Decanol (CAS) $$ 2-Hydroxydecane $$ Methyl-n-oct... 45

5000 A 4.80 5.00 5.20 5.40 27 m/z 41.10 17.29% 57 69 83 n A miz-> 0- 20 30 40 HL 50 60 70 97 112 - ■ i • ■ 1,1 i ■ ■ ■ ■ i 1 ‘ ■ i ' ■ • ' i ■ 80 90 100 110 120 130 140 140 \ Abundance #40801: 2-Nonanol 45

4.80 5.00 5.20 5.40 ‘ ‘

w_ 5000 m/z 43.10 16.57%

27 69 -H -PPP 84 56 98 111

_N 0- ■ i ■ i ■ ■i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ‘ ■ i ■ ■ ■ ■ i ■ ■ miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #78514: n-Hexyl lactate 45 4.80 5.00 5.20 5.40 m/ z 55.10 16.27%

5000

56 69 84 0 । । ■ ■ ■ ■ ।. ■ ■ ■ । I ■ ' 1 ' 11 ■ i' I ■ i ■ ■ ■ ■ i ■' ■ ■ i • ■ ■ ■ i ■ ■ ■ • i ■ ■ ■ ■ i ■ 1 ■ ■ i' ■ ■ ■ i ■ ■ ■ ।' ■1 f 1 ‘1 ■ । ■ ■ ‘' । ■ ‘ ■ ■ । n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 4.80 5.00 .5.20 5.40

01508.D HP022102.M Mon Feb 25 10:54:57 2002 Page 8

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