GCMS analysis results for sample AD29522, Feb 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB01\29522.D Vial: 4 Acq On : 1 Feb 2002 1:04 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 2-Propanol, 1- (2-methoxypro. .. Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

9.86 0.07 ug/L 30865 1,4-Dichlorobenzene-d4 9.71

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxypropoxy)... 148 C7H16O3 013429-07-7 74 2 Butanoic acid, 2-hydroxy- $$ But... 104 C4H803 000565-70-8 39 3 3-Heptanol (CAS) $$ 3-Hydroxyhep... 116 C7H160 000589-82-2 9 4 Silane, ethenyltrimethyl- (CAS) ... 100 C5H12Si 000754-05-2 9 Abundance Scan 568 (9.858 min): 29522.D (-) m/z 59.10 100.00% 59

5000

45 86 73 104 ML... 9.60 9.80 10.00 10.20 Of ' I ‘ ‘ 1 * 1 • • i J । । . • , < । — . [-m-T-p m/z 45.10 17.00% miz->. 20 30 40 50 60 70 801 90 100 110 120 130 Abundance #43942: 2-Propanol, 1-(2-methoxypropoxy)-$$ 1-(2-Methoxyp... 59 1

5000 9.60 9.80 10.00 10.20 m/z 43.10 12.47% 31 45

miz-> Of 20 -. 4 „. —194.. 130. 30 40 50 60 70 80 90 100 110 120 130 A Abundance #10063: Butanoic acid, 2-hydroxy- $$ Butyric acid, 2-hydro... 31 59 TT 1111 TEImr 9.60 9.80 10.00 10.20 5000 m/z73.10 11.48% 45 76 104 01 ■ i' ■ II8 11' i1 ++ i'1 • ■ i ■ • ■ i ‘ 1 ' ■ i ■ ' ■ ‘ i ■ ' ■ ■ i ■ ' 1 ' i ' ' ‘ ■ i ■ '

miz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #16981: 3-Heptanol (CAS) $$ 3-Hydroxyheptane $$ 1 -Ethyl-1 —ANAA.... 9.60 9.80 10.00 10.20 m/z41.10 8.78% 69 5000 31 41

87

m/z-> 0, -H— 20 30 40 50 1 i • ' ■ ‘ I ''■ ■ ■ i ■ 1 ‘ 1 i • ■ ■ ■ i ' ■ ' ■ i 1 ■ ■ ■ i • ■ ■ ■ i ■ ■

60 70 80 90 100 110 120 130 9.60 "I[ • • i ■ • 9.80 10.00 10.20

29522.D SCAN508.M Mon Feb 04 08:41:11 2002 Page 6

NYC-WTC_000036788