GCMS analysis results for sample AE00473, Jan 18 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN10\00466 .D Vial: 4 Acq On 10 Jan 2002 5:18 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxypro... Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 9.86 0.17 ug/L 57059 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxypropoxy)... 148 C7H16O3 013429-07-7 64 2 3-Heptanol (CAS) $$ 3-Hydroxyhep... 116 C7H160 000589-82-2 33 3 N-(2-lsopropoxy-2-methyl-l-propy ... 185 C11H23NO 132555-83-0 33 4 3-Heptanol, 4-methyl- $$ 4-Methy... 130 C8H180 014979-39-6 33 Abundance Scan 568 (9.858 min): 00466.D (-) m/z 59.10 100.00% 59

5000

0 1 ■ i 1 41

,.14.51, RI 73 ........... I I ’ ' ' ' I ’ ’ 84 ----- 104 136 m/Z /LU 9.60 55.10 9.80 A -N 10.00 10.20 33.57% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 .A Abundance #43942: 2-Propanol, 1-(2-methoxypropoxy)- $$ 1-(2-Methoxyp... 59

5000 A 9.60 9.80 10.00 10.20 m/z 41.10 13.63%

/z-> 0- 31 ----4 3060 _13 70 80 45

90 100 110 120 130 140 40 50 73 104 ' i 1 ■ ■ 1 i ' ■ ' 1 i ' ' ' 1 i ■ 1 ' ' i ' ■ ' ' i ' ' 1 ' i ' 1 ' ' i 1 ‘ A A Abundance #16993: 3-Heptanol (CAS) $$ 3-Hydroxyheptane $$ 1-Ethyl-1-... 59 69 1 ' i 9.60 9.80 10.00 10.20 5000 m/z 45.10 12.55% 41 87

98 0- 1 T-r-p-i-r-r^T 1Pt ■ I ■ ■ । 1 i 1 1 1 1 i ' 1 1 1 i 1 1 ■ ■ i ■ ' ■ ' i ■ ■ ■ 1 i ■ ■ m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #94047: N-(2-lsopropoxy-2-methyl-1-propylidene)t-butylamin... ' ■ i ' ' 1 ■ i ' ' ■ i ' 1 ■ ' i 1 ■ 59 960 9.80 10.00 10.20 m/z 43.10 11.34%

5000 J

42 0 9 1 ■ i 1 1 ' 1 1' 1 1 1 1 1 TIit 70 84 101 112 127 - TT ■ ' i 1 1 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 9.60 9.80 10.00 10.20

0466.D SCAN508.M Fri Jan 11 10:08:36 2002 Page 4

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