GCMS analysis results for sample AE00473, Jan 18 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN10\00466.D vial: 4 Acq On 10 Jan 2002 5:18 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P pot A (ovy Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Azou Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 1,4-Dimethyl-3,5-propanobic... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 18.73 2.88 ug/L 1526220 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qua 1

1 1,4-Dimethyl-3 ,5-propanobicyclo[... 192 C13H20O 000000-00-0 37 2 Benzo[l,2-c:4,3-c]bis(isothiazol... 192 C8H4N2S2 074960-06-8 9 3 2,4 (1H, 3H) -Quinazolinedione , 3-h... 192 C9H8N203 037833-99-1 9 4 Benzo[1,2-c:3,4-c]bis(isothiazol... 192 C8H4N2S2 074960-05-7 9 Abundance Scan 1345 (18.729 min): 00466.D (-) m/z 191.80 100.00% 64 192

5000 128 96 18.40 18.60 18.80 19.00 36 44 .1 76 86 | , 160 180 0 V' '1 [ '"I "" I1 .............Batpovvr +r 111" " i " 1' i " 1111T1 1111 ■ 11 ■ > ■ > ■ m/ Z 64.00 90.45% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103601:1,4-Dimethyl-3,5-propanobicyclo[2.2.2]octan-2-one 107 192

119 159 93 5000 132 145 18.40 18.60 18.80 19.00 174 m/z 127.90 33.86%

m/z-> 0 ■ ।"111 ■ ■ ■11 ■'' ■ । ■111'1" ।1

Abundance /‘‘‘‘ J 1 1 1 1 I 1 11 1 I ■' r ' " r ' 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200

5000 45 #102105: Benzo[1,2-c:4,3-c]bis(isothiazole) $$ Benzo[1,2-c...

69 T-p-r

148 |... -P

165 192 _y 18.40 18.60 18.80 19.00 m/z 193.80 25.70% TT

96 121 Of r i " '' i' " 11' " ' i'1 1 ■ i ■ ■ ■ ■ । • > I > 11 ■ ■ > । ■ i ■ • ■. । . i ■. T‘ ' " I " 1' i " " i " " i 1" i " m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102266: 2,4(1 H,3H)-Quinazolinedione, 3-hydroxy-1-methyl- 192 18.40 18.60 18.80 19,00 92 m/ Z 95.90 14.63% 132 5000 104 162 77 176

n/z-> 0 mm 119 TIIT 111 ■'" i ■1 ■ ■ I 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 । 148 ____ L ‘ ITTi ' i1" ' i "rr 1 ' i ' ■ 18,40 18.60 18.80 19.00

30466.D SCAN508.M Fri Jan 11 10:08:36 2002 Page 5

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