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GCMS analysis results for sample AE00473, Jan 18 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00473 conducted on January 18, 2002.

NYC-WTC_000051283–000051300

Folder label: “GCMS X 1/8/02 A 1/10/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C : \MSDCHEM\1\5973N\02JAN10\00466 . D Vial: 4 Acq On 10 Jan 2002 5:18 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 4 bis(2-furyl)dimethylsilane Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 20.93 0.12 ug/L 71353 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual,

1 bis(2-furyl)dimethylsilane 192 C10H12O2Si 000000-00- 9 2 1-Allyl-3-phenyl-2-thiourea 192 C10H12N2S 000000-00-0 A(c- 3 3-(2,2,5,5-Tetramethyl-pyrrolid-... 192 C11H16N2O 000000-00-0 9 4 1-(2-Propenyl)-la,9b-dihydrophen... 233 C17H15N 091540-30-6 9 Abundance Scan 1538 (20.933 min): 00466.D (-) m/z 177.10 100.00% 177 41 64 221 192 5000 96 163 233 248

128 0 'I 1 - 1 ' r | 20.60 20.80 21.00 21.20 0- 1 1 i ■ 1 T I m/z 41.10 72.35% m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #102523: bis(2-furyl)dimethylsilane v 177

192 5000 149 ' ' I 1 1 1 1 I 1 1 1 1 1 1 ' ' 1 1 1 1I 20.60 20.80 21.00 21.20 43 m/z 64.00 72.09% 95 , , II........... J.... ............ I 0- IIIII+IIIIIIT _/ m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #102518:1 -Allyl-3-phenyl-2-thiourea 41 93

51 77 177 20.'60 20.80 21.00 21.20 5000 65 192 m/z 221.10 61.56%

118 136 159 0— - m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #102861: 3-(2,2,5,5-Tetramethyl-pyrrolid-3-onyl)-acrylonitril 93 109 177 20.60 20.80 21.00 21.20 m/z 191.80 53.45% 192 5000 42

52 66

/z-> 0 — . ...... - 40 60 80 100 . . 17212 . 120 140 160 180 200 220 240 20.60 20.80 21.00 21.20

00466.D SCAN508.M Fri Jan 11 10:08:36 2002 Page 6

NYC-WTC_000051292

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NYC-WTC_000051292Source: NYC Law Department, mirrored locally

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