Laboratory report showing non-detect levels for 15 volatile organic compounds in a GCMS method blank processed on May 23, 2002.
NYC-WTC_000025347–000025358Folder label: “GCMS X 5/16/02 A 5/20/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C : \MSDCHEM\ 1 \DATA\ 052002\516LBL. D Vial: 4 Acq On : 20 May 2002 3:44 pm Operator: Mclean Sample : 5/16 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L
Peak Number 4 4-Hydroxy-3,5-dimethylcinna ... Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T. 22.58 0.24 ug/L 238555 Phenanthranene-dl0 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 4-Hydroxy-3 ,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 50 2 2,5-Dihydrophosphole, 3-methyl-1... 192 C11H13OP 1000196-97-5/45 3 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 42 ) 4 3-(2-Methoxy-5-methylphenyl)acry... 192 C11H1203 103986-76-1 42 7 Abundance Scan 3319 (22.580 min): 516LBL.D (-3304) (-) m/z 192.10 ioo .oo%| 192
5000
,............ ..........................
40 22 66.“ 96I 120 146 160 22.20 22.40 22.60 22.80 23.00 0 TPWWTTIWTTTTTTTTTTTTTTHHTTTTTTTTTTHTTTTTTTTTTTTT 111" '1111 "'I'" 11' " 1 r 1 " I m/z 191.00 21.00%| m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81030: 4-Hydroxy-3,5-dimethylcinnamic acid 192
5000 ' 1 1 1 1 1 1 r' ' "I" 22.20 22.40 22.60 22.80 23.00 89 175 m/z 193.00 15.15%| 63 117 145
O+ 45 | 77 105 1| TTTTTTT 135 | 163 4 n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80965: 2,5-Dihydrophosphole, 3-methyI-1-oxo-1-phenyl- 192 164 ■ l ■ ■ ■ ■ I ■ • 1 1 1 1 ' 1 1 i ‘ 22.20 22.40 22.60 22.80 23.00 5000 99 m/z 146.10 13.88% 115 47 77 177 67 125,34 146 mfe-> 0 27 3 1.57 || - +87+ 4+155, HHI 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 _________ . Abundance #81033: Phenanthrene, 9-methyl- 192 22.20 22.40 22.60 22.80 23.00 m/z 96.10 13.21%| 5000
96
m/z-> 29 39 51 63 74 83 ,11 1 ' I 115 0 TIOIImpnnOUTT Immampr 126 139 152 165 176 1 ‘ 1 1 [ ' 1 1 ' I * ' ‘ '‘l 1 “ 1 I'1 " ' I 4TTTHTT 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 U ' I ' ' ' ' I ' ' 22.20 22.40 22.60 22.80 23.00 1 1 1 1 1 ' ‘ I '
516LBL.D 050102.M Wed May 22 15:57:33 2002 Page 6
NYC-WTC_000025356
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NYC-WTC_000023843
Laboratory report showing non-detectable levels of nitrosamines and other contaminants in a GC/MS blank sample AE10901.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024153
Document noting low recovery in GCMS scan of sample AE10205 and subsequent re-extraction yielding 85% recovery.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023502
Laboratory report showing GC/MS analysis results for sample AE10816 including surrogate recovery data on May 14, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022795
GCMS analytical report for environmental sample AE09151 including surrogate compound data from May 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025054
Laboratory report showing GCMS blank analysis for sample AE11379 conducted on May 21, 2002, with results below minimum reporting levels.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023531
Laboratory report page showing GC/MS analysis for sample AE10850 including surrogate recovery data on May 14, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025447
Laboratory report showing GCMS results for sample AE11421 analyzed on May 30, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022719
Laboratory report showing non-detect levels for various volatile organic compounds in a method blank.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023439
Laboratory report showing GC/MS analysis results for sample AE10137 including surrogate recovery data on May 14, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022763
GCMS analytical report for environmental sample AE09331 including surrogate compound data from May 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045048
Laboratory report showing blank analysis results for volatile organic compounds in sample AE10303 on May 9, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043869
Laboratory blank report for sample AE09771 showing non-detectable levels of target compounds from May 8, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000025344
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
Filed in the same folder
NYC-WTC_000025345
Laboratory log sheet recording Method 608 extraction parameters and sample counts for DEP testing in May 2002.
Filed in the same folder
NYC-WTC_000025359
Laboratory report of GCMS calibration data showing response values and detection limits for 15 volatile organic compounds on May 23, 2002.
Filed in the same folder
NYC-WTC_000025363
Laboratory report of GCMS reference standard analysis showing response values for 15 volatile organic compounds on May 23, 2002.
Filed in the same folder
NYC-WTC_000025371
Laboratory report of GCMS analysis for sample AE11417 conducted on May 30, 2002, showing surrogate recovery data.
Filed in the same folder