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GCMS blank analysis results for sample AE11417, May 2002

Machine-extracted title · confidence 100%

Laboratory report showing non-detect levels for 15 volatile organic compounds in a GCMS method blank processed on May 23, 2002.

NYC-WTC_000025347–000025358

Folder label: “GCMS X 5/16/02 A 5/20/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C : \MSDCHEM\ 1 \DATA\ 052002\516LBL. D Vial: 4 Acq On : 20 May 2002 3:44 pm Operator: Mclean Sample : 5/16 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Anthracene-dlO- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 23.11 0.39 ug/L 382798 Phenanthranene-dl0 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-diO- 188 C14D10 001719-06-8 87 ‘ 2 Phenanthrene-diO 188 C14D10 001517-22-2 50- 3 Antipyrine 188 C11H12N20 000060-80-0 33 4 Pentacyclo[7.3.1.1.(4,12).0(2,7)... 188 C14H20 1000215-61-8 9 Abundance Scan 3409 (23.109 min): 516LBL.D (-3402) (-) m/z 188.10 ioo.oo%| 188

5000 ........./.................................. 94 1 ' i 1 ' ■ 1 i 1 ' 1 1 i ' 1 ■ 1 1777 1 1 1 57 66 80 156 | 22.80 23.00 23.20 23.40 0 ' I "1' 1111' I " " I'11 '‘l1'llf I " •111 ■ i1 ■" i■1■■i'1 > ■ i T’’ mm m/z 94.05 17.42%| m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 ....................................... .. . . . 22.80 23.00 23.20 23.40 m/z 189.10 14.74% RR 80 94 160 , 17 30 42 52 ° J J 108 118 132 146 I ■ I170179/ 01 । | I । ' I | I < ' I | < i * i | I I > I [ I I I 1 [ I I I I | I | I I [ I | i t"| TTl"l | 1 1 I I | I J I I | I J I I ] I I I ! JI T t r J r f I | I I I J | I1)1! I | Illi

m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

22.80 23.00 23.20 23.40 5000 m/z 184.00 14.16%|

80 94 160 30 42 52 66 108 118 132 146 I 170179 OT TTT t-11111111111111111 [ 11 H 111 1 | | I I 1 I | I I 1 I j I I I I | I I I I | I I I I | I I I I [ I rl'l |’l I I I"] I 1 I 1 | P| rl | Illi

m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #125688: Antipyrine ............................................ 188 22.80 23.00 23.20 23.40 96 m/ z 80.05 9.91%|

5000 n 56 105

/z-> 0 —2 +1+ TH 68 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 । 115 129 145 159 1/3 | . ................... 'I ""I'1........ 1 TTT 22.80 23.00 23.20 23.40

516LBL.D 050102.M Wed May 22 15:57:36 2002 Page 7

NYC-WTC_000025357

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NYC-WTC_000025357Source: NYC Law Department, mirrored locally

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