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GCMS sample analysis results, AE11902, June 3, 2002

Machine-extracted title · confidence 100%

Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11902.

NYC-WTC_000012881–000012907

Folder label: “GCMS X 5-21-02 A 5-22-02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C: \MSDCHEM\ 1 \DATA\ 052202\11902.D Vial: 9 Acq On : 22 May 2002 8:20 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 18 Anthracene-dlO- Concentration Rank 17 R.T. EstConc Area Relative to ISTD R.T. 23.07 0.22 ug/L 208996 Phenant hranene-d10 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-diO- 188 C14D10 001719-06-8 87 2 Phenanthrene-diO 188 C14D10 001517-22-2 74— 3 1,4-Naphthalenedione, 2-hydroxy-... 188 C11H8O3 000483-55-6 38 4 Pentacyclo[8.4.0.0(3,7).0(4,14).... 188 C14H20 1000099-27-2 33 Abundance Scan 3402 (23.068 min): 11902. D (-3396) (-) m/z 188.10 100.00% 188

5000

94 -- 80 160 22.80 23.00 23.20 23.40 49 0 TWApgTp i ■ “' m/ Z 94.10 20.48% niz-> 10 2030405060 70 8090 100110120130140150160170180190 Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/z 189.10 20.06% 80 94 160 17 30 42 52 66 108118 132 146 ,| , |.I 170179.1,1 0 ((।. .1 |! ,. > । n > > TH 11111 Hn [I I H | ll 11 111 n | 11 111 u r>| ll I'I'I'l 11 I 1111 1 | I’l’t’t Illi miz-> 10 20 30 40 50 60 70 80 90 100110120130140150 160170180190 Abundance #79827: Phenanthrene-d10 188

22.80 23.00 23.20 23.40 5000 m/z 184.10 15.09%

80 160

tn/z~> 30 42 52 66 0 TPOt 14 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 108118 132 146 1' H11»I ■ i~»; ■ > 111 H11» 46—14170179— ) Abundance #125707:1,4-Naphthalenedione, 2-hydroxy-3-methyl- 1 188 22.80 23.00 23.20 23.40 m/z 80.00 14.88%

5000

77 105 131 160 50 0 ......... .■■■■I'..'.. , I ,.[1ri ... I ri I I 11 I 11'1'11 I n-n pni 1I’’ ...................... i 11 11 i 11 l 11 i''! T' '1 ' |'11 | ‘* r "■ ........... H___________

m/z-> 10 2030405060 70 8090 100110120130140150 160 170 180 190 22.80 23.00 23.20 23.40

11902.D 052202.M Tue May 28 12:06:51 2002 Page 21

NYC-WTC_000012906

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NYC-WTC_000012906Source: NYC Law Department, mirrored locally

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