GCMS analysis results for sample AE11419, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\052002\11419.D Vial: 9 Acq On : 20 May 2002 7:48 pm Operator: Mclean Sample : 5/16 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.38 ug/L 385200 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual A 1 Anthracene-dlO- 188 C14D10 001719-06-8 72) 2 Phenanthrene-diO 188 C14D10 001517-22-2 450 3 4H-Pyrido[1,2-a]pyrimidin-4-one,... 188 C11H12N2O 057773-19-0 40 4 Pentacyclo[7.3.1.1. (4,12) .0(2,7) ... 188 C14H20 1000215-61-8 36 Abundance Scan 3409 (23.109 min): 11419.D (-3403) (-) m/z 188.10 100.00% US

5000 .......................... ................. ........... 80 94 158 । 22.80 23.00 23.20 23.40 .......... 44 54 66 0 '> 11 > ■ > 11 >' ■ 11 ■1111«■ i [ H >1;. 11.11 i.... > I ''" I । 11 ■ ■ H11. ■ < ।।. pi1 T’TT m/z 189.15 22.30%| m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- US

------- 5000 22.80 23.00 23.20 23.40 m/ z 94.10 17.00% 17 30 42 52 66 0 ' r 1" i " " I" H l1" ■ i111 11111111111111111 80 94 108 118 132 । । ] 1 r 11 11 i 11 111 i! 1111 1‘ 160 146—4-179179— , . fl mfe-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 ......... ............. .............................. 1111’+ 11/14 I4++I‘‘‘‘I 22.80 23.00 23.20 23.40 5000 m/z 80.00 14.05%

80 94 160 O-p 30 42 52 66 11 108 118 132 11" ■ ■ 1" " 111" । " I ■ l ■ ■ bl | " "I I I I I | t 1 I I [ I 1 1 T | I T I 1 pl 1 1 I 146—4179179 n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79770: 4H-Pyrido[1,2-a]pyrimidin-4-one, 3-ethyl-6-methyl- 145 1tS 22.80 23.00 23.20 23.40 173 m/z 184.10 14.05%

5000 92

65 39 159

/z-> I, 55 . HH I 78 | 0 1 r " 1111111'1 ■ p ■ ■ ■ |‘l‘s ■ i I’ 1111-1I 1I '''111111'11 ‘ 111 1111' 11''' 111 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 119 132 ‘p-rrr ................ ........................ ............ 22.80 23.00 23.20 23.40

11419.D 050102,M Thu May 23 10:46:57 2002 Page 8

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