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GCMS blank analysis for sample AE10303, May 2002

Machine-extracted title · confidence 100%

Laboratory report showing blank analysis results for volatile organic compounds in sample AE10303 on May 9, 2002.

NYC-WTC_000045048–000045062

Folder label: “GCMS X 5/1/02 A 5/8/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C: \MSDCHEM\1\DATA\050802\0501LB.D Vial: 3 Acq On 8 May 2002 3:26 pm Operator: Mclean Sample 5/1 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 4 2,5-Dihydrophosphole, 3-met.. Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 22.58 0.27 ug/L 310494 Phenanthranene-dlO 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,5-Dihydrophosphole, 3-methyl-1... 192 C11H13OP 1000196-97-5 5 2 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 45 3 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5/42 4 Phenanthrene, 2-methyl- ____ 192 C15H12 002531-84- 2 40 Abundance “Scan 3319 (22.580 min): 0501 LB.D (-3311) (-) m/z 192.10 10 . 00% 192

5000

96 146 I I ' I I I I I I I I I I I I I J I I 'l I I I

160 22.20 22.40 22.60 22.80 23.00

m/z-> 40 70 82 i 118 O' I J I I F T | I I I I I I I I | I I 1 > | I > I > | I I I I | I I I I TTTTTTTTTTTTTTTTTTTTT> । *

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 gag* U m/ z 191.10 21.33%| Abundance #80965: 2,5-Dihydrophosphole, 3-methyl-1-oxo-1-phenyl- 192 164

5000 99 । 1 ' ' ' । 1 ■ । । ( 1 1 1 1 r 1 1 1 । 1 115 22.20 22.40 22.60 22.80 23.00 47 77 177 m/ z 146.00 17.40%| 67 125 134 146 27 38, , 1,57 a 17.7+ ++ lpsil.ljpotm171r.155,. 11111 IIp 1" f 11310 0 I | I I I I | I I I r| I I I I | I I I I | ri I I | TH+ ...’ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80953: 2-Propenal, 3-(3,4-dimethoxyphenyl)- 192 161 ,1....... 22.20 22.40 22.60 22.80 23.00 5000 m/ z 96.10 16.25%| 77 91 121 149 177 103 138 0 11 ‘111111 r' i 52 641111 > /II । ■11 I n r'। । losglalgoo I— 111" '11 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 1 । । i”I | । । L _ | r Abundance #81033: Phenanthrene, 9-methyl- 1 1 1 ' 192 22.20 22.40 22.60 22.80 23.00 m/z 193.10 14.43%|

5000

96

m/z-> 29 39 51 63 74 83 II 115 126 139 152 0 * ।1'' ■ । *1111111111101—' ’TTT’i' r[l'111 Fl11 ■1 T1’010000"0"003T—mr 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 +176 I. I 165 Tri mltij T’1’ 22.20 22.40 22.60 22.80 23.00

0501LB.D 050102.M Thu May 09 13:47:15 2002 Page 7

NYC-WTC_000045058

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NYC-WTC_000045058Source: NYC Law Department, mirrored locally

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